Physics of the Solid State

, Volume 59, Issue 4, pp 784–790 | Cite as

Structure and physical properties of iron nanotubes obtained by template synthesis

  • A. E. Shumskaya
  • E. Yu. Kaniukov
  • A. L. Kozlovskiy
  • M. V. Zdorovets
  • V. S. Rusakov
  • K. K. Kadyrzhanov
Low-Dimensional Systems


Iron nanotubes with an aspect ratio of approximately 100 are synthesized by electrochemical deposition using polyethylene terephthalate templates. The structural and morphological features of the nanotubes are studied in detail by scanning electron microscopy, energy dispersive analysis, transmission electron microscopy, electron diffraction, X-ray diffraction analysis, and gas permeability. The main magnetic parameters and their dependence on temperature are determined by vibration magnetometry and Mössbauer spectroscopy.


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  1. 1.
    D. T. Mitchell, S. B. Lee, L. Trofin, N. Li, T. K. Nevanen, H. Söderlund, and C. R. Martin, J. Am. Chem. Soc. 124, 11864 (2002).CrossRefGoogle Scholar
  2. 2.
    S. K. Yen, P. Padmanabhan, and S. T. Selvan, Theranostics 3, 986 (2013).CrossRefGoogle Scholar
  3. 3.
    B. Kalska-Szostko, E. Orzechowska, and U. Wykowska, Colloids Surf., B 111, 509 (2013).CrossRefGoogle Scholar
  4. 4.
    M. Safi, M. Yan, M. A. Guedeau-Boudeville, H. Conjeaud, V. Garnier-Thibaud, N. Boggetto, A. Baeza-Squiban, F. Niedergang, D. Averbeck, and J. F. Berret, ACS Nano 5, 5354 (2011).CrossRefGoogle Scholar
  5. 5.
    S. R. Dave and X. Gao, Wiley Interdiscip. Rev.: Nanomed. Nanobiotechnol. 1, 583 (2009).Google Scholar
  6. 6.
    C. R. Martin, Science (Washington) 266, 1961 (1994).ADSCrossRefGoogle Scholar
  7. 7.
    L. Dauginet-De Pra, E. Ferain, R. Legras, and S. Demoustier-Champagne, Nucl. Instrum. Methods Phys. Res., Sect. B 196, 81 (2002).ADSCrossRefGoogle Scholar
  8. 8.
    E. Y. Kaniukov, J. Ustarroz, D. V. Yakimchuk, M. Petrova, H. Terryn, V. Sivakov, and A. V. Petrov, Nanotechnology 27, 115305 (2016)ADSCrossRefGoogle Scholar
  9. 9.
    L. G. Vivas, Y. P. Ivanov, D. G. Trabada, M. P. Proenca, and O. Chubykalo-Fesenko, Nanotechnology 24, 105703 (2013).ADSCrossRefGoogle Scholar
  10. 10.
    Y. A. Ivanova, D. K. Ivanov, A. K. Fedotov, E. A. Streltsov, S. E. Demyanov, A. V. Petrov, E. Y. Kaniukov, and D. Fink, J. Mater. Sci. 42, 9163 (2007).ADSCrossRefGoogle Scholar
  11. 11.
    V. Haehnel, S. Fähler, P. Schaaf, M. Miglierini, C. Mickel, L. Schultz, and H. Schlörb, Acta Mater. 58, 2330 (2010).CrossRefGoogle Scholar
  12. 12.
    L. Boarino, S. Borini, and G. Amato, J. Electrochem. Soc. 156, K223 (2009).CrossRefGoogle Scholar
  13. 13.
    J. Qin, J. Nogués, M. Mikhaylova, A. Roig, J. S. Muñoz, and M. Muhammed, Chem. Mater. 17, 1829 (2005).CrossRefGoogle Scholar
  14. 14.
    S. E. Demyanov, E. Y. Kaniukov, A. V. Petrov, E. K. Belonogov, E. A. Streltsov, D. K. Ivanov, Y. A. Ivanova, C. Trautmann, H. Terryn, M. Petrova, J. Ustarroz, and V. Sivakov, J. Surf. Invest. 8, 805 (2014).CrossRefGoogle Scholar
  15. 15.
    Z. Hua, S. Yang, H. Huang, L. Lv, M. Lu, B. Gu, and Y. Du, Nanotechnology 17, 5106 (2006).ADSCrossRefGoogle Scholar
  16. 16.
    D. Zhou, T. Wang, M. G. Zhu, Z. H. Guo, W. Li, and F. S. Li, J. Magnetics 16, 413 (2011).CrossRefGoogle Scholar
  17. 17.
    X. F. Han, Z. C. Wen, and H. X. Wei, IEEE Trans. Magn. 47, 2957 (2011).ADSCrossRefGoogle Scholar
  18. 18.
    H. Hillebrenner, F. Buyukserin, J. D. Stewart, and C. R. Martin, Nanomedicine (London) 1, 39 (2006).CrossRefGoogle Scholar
  19. 19.
    S.-H. Liao, K.-L. Chen, C.-M. Wang, J.-J. Chieh, H.-E. Horng, L.-M. Wang, C. Wu, and H.-C. Yang, Sensors 14, 21409 (2014).CrossRefGoogle Scholar
  20. 20.
    B. Tylkowski and I. Tsibranska, J. Chem. Technol. Metall. 50, 3 (2015).Google Scholar
  21. 21.
    B. Yoo, F. Xiao, K. N. Bozhilov, J. Herman, M. Ryan, and N. V. Myung, Adv. Mater. 19, 296 (2007).CrossRefGoogle Scholar
  22. 22.
    M. Motoyama, Y. Fukunaka, T. Sakka, and Y. H. Ogata, Electrochim. Acta 53, 205 (2007).CrossRefGoogle Scholar
  23. 23.
    T. N. Narayanan, M. M. Shaijumon, L. Ci, P. M. Ajayan, and M. R. Anantharaman, Nano Res. 1, 465 (2008).CrossRefGoogle Scholar
  24. 24.
    C. Schönenberger, B. M. I. van der Zande, L. G. J. Fokkink, M. Henny, C. Schmid, M. Krüger, A. Bachtold, R. Huber, H. Birk, and U. Staufer, J. Phys. Chem. 101, 5497 (1997).CrossRefGoogle Scholar
  25. 25.
    M. Motoyama, Y. Fukunaka, T. Sakka, Y. H. Ogata, and S. Kikuchi, J. Electroanal. Chem. 584, 84 (2005).CrossRefGoogle Scholar
  26. 26.
    E. Kaniukov, A. Kozlovsky, D. Shlimas, D. Yakimchuk, M. Zdorovets, and K. Kadyrzhanov, Inst. Phys. Conf. Ser.: Mater. Sci. Eng. 110, 012013 (2016).Google Scholar
  27. 27.
    C. Guillén and J. Herrero, Thin Solid Films 480, 129 (2005).ADSCrossRefGoogle Scholar
  28. 28.
    M.E. Toimil-Molares, Beilstein J. Nanotechnol. 3, 860 (2012).CrossRefGoogle Scholar
  29. 29.
    M. Krajewski, W. S. Lin, H. M. Lin, K. Brzozka, S. Lewinska, N. Nedelko, A. Slawska-Waniewska, J. Borysiuk, and D. Wasik, Beilstein J. Nanotechnol. 6, 1652 (2015).CrossRefGoogle Scholar
  30. 30.
    S. Yang, H. Zhu, D. Yu, Z. Jin, S. Tang, and Y. Du, J. Magn. Magn. Mater. 222, 97 (2000).ADSCrossRefGoogle Scholar
  31. 31.
    H. Zeng, R. Skomski, L. Menon, Y. Liu, S. Bandyopadhyay, and D. J. Sellmyer, Phys. Rev. B: Condens. Matter 65, 134426 (2002).ADSCrossRefGoogle Scholar
  32. 32.
    M. Almasi Kashi, A. Ramazani, and A. S. Esmaeily, IEEE Trans. Magn. 49, 1167 (2013).ADSCrossRefGoogle Scholar
  33. 33.
    D. J. Sellmyer, M. Zheng, and R. Skomski, J. Phys.: Condens. Matter 13, R433 (2001).ADSGoogle Scholar

Copyright information

© Pleiades Publishing, Ltd. 2017

Authors and Affiliations

  • A. E. Shumskaya
    • 1
  • E. Yu. Kaniukov
    • 1
  • A. L. Kozlovskiy
    • 2
    • 3
  • M. V. Zdorovets
    • 2
    • 4
    • 5
  • V. S. Rusakov
    • 6
  • K. K. Kadyrzhanov
    • 3
  1. 1.Scientific and Practical Material Research CentreNational Academy of Sciences of BelarusMinskBelarus
  2. 2.Institute of Nuclear Physics of the Republic of KazakhstanAlmatyKazakhstan
  3. 3.Gumilyov Eurasian National UniversityAstanaKazakhstan
  4. 4.Ural Federal UniversityYekaterinburgRussia
  5. 5.National Research Nuclear University “MEPhI”MoscowRussia
  6. 6.Moscow State UniversityMoscowRussia

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