Skip to main content
Log in

Differential scanning calorimetry study of the phase transition in diserine sulfate monohydrate crystals

  • Lattice Dynamics and Phase Transitions
  • Published:
Physics of the Solid State Aims and scope Submit manuscript

Abstract

Differential scanning calorimetry (DSC) was used under the highest resolution conditions to study the phase transition in diserine sulfate monohydrate crystals. In the temperature range 255–270 K, the DSC signal was found to exhibit sharp Λ-shaped peaks with a thermal hysteresis of 8.5 K, which indicates the occurrence of a first-order phase transition. The experimental data are used to determine the thermodynamic parameters of the phase transition.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. V. V. Lemanov, S. N. Popov, V. V. Bakhurin, and N. V. Zaĭtseva, Fiz. Tverd. Tela (St. Petersburg) 43(7), 1283 (2001) [Phys. Solid State 43 (7), 1336 (2001)].

    Google Scholar 

  2. Yu. I. Smolin, A. E. Lapshin, and I. A. Drozdova, Fiz. Tverd. Tela (St. Petersburg) 44(10), 1881 (2002) [Phys. Solid State 44 (10), 1972 (2002)].

    Google Scholar 

  3. V. K. Yarmarkin, S. G. Shul’man, and V. V. Lemanov, Fiz. Tverd. Tela (St. Petersburg) 48(8), 1482 (2006) [Phys. Solid State 48 (8), 1568 (2006)].

    Google Scholar 

  4. V. A. Bershtein and V. M. Egorov, Differential Scanning Calorimetry of Polymers: Physics, Chemistry, Analysis, and Technology (Khimiya, Leningrad, 1990; Ellis Horwood, New York, 1994).

    Google Scholar 

  5. K. Illers, Eur. Polym. J. 10, 911 (1974).

    Article  Google Scholar 

  6. L. D. Landau and E. M. Lifshitz, Course of Theoretical Physics, Vol. 5: Statistical Physics (Nauka, Moscow, 1976; Pergamon, Oxford, 1980).

    Google Scholar 

  7. I. Hatta and A. Ikushima, J. Phys. Chem. Solids 34, 57 (1973).

    Article  Google Scholar 

  8. J.-M. Martin-Olalla, S. Ramos, and A. Levanyuk, Phys. Rev. B: Condens. Matter 39, 14265 (1999).

    Google Scholar 

  9. J.-M. Martin-Olalla, J. del Cerro, and S. Ramos, J. Phys.: Condens. Matter 12, 1715 (2000).

    Article  ADS  Google Scholar 

  10. G. Dolino, J. P. Bachheimer, and C. M. E. Zeyen, Solid State Commun. 45, 295 (1983).

    Article  Google Scholar 

  11. T. A. Aslanyan and A. P. Levanyuk, Solid State Commun. 31, 547 (1979).

    Article  Google Scholar 

  12. J. Durand, M. Lopez, L. Cot, O. Retout, and P. Saint-Gregoire, J. Phys. C: Solid State Phys. 16, L311 (1983).

    Article  ADS  Google Scholar 

  13. J. P. Bachheimer, B. Berge, G. Dolino, P. Saint-Gregoire, and C. M. E. Zeyen, Solid State Commun. 51, 55 (1984).

    Article  Google Scholar 

  14. V. M. Egorov, B. I. Smirnov, V. V. Shpeĭzman, R. K. Nikolaev, and N. S. Sidorov, Fiz. Tverd. Tela (St. Petersburg) 47(10), 1914 (2005) [Phys. Solid State 47 (10), 1993 (2005)].

    Google Scholar 

  15. B. M. Strukov and I. V. Shnaĭdshteĭn, private communication.

Download references

Author information

Authors and Affiliations

Authors

Additional information

Original Russian Text © V.M. Egorov, V.V. Lemanov, 2006, published in Fizika Tverdogo Tela, 2006, Vol. 48, No. 10, pp. 1838–1842.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Egorov, V.M., Lemanov, V.V. Differential scanning calorimetry study of the phase transition in diserine sulfate monohydrate crystals. Phys. Solid State 48, 1954–1958 (2006). https://doi.org/10.1134/S1063783406100234

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1063783406100234

PACS numbers

Navigation