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Atom Probe Tomography of High-Entropy Alloy AlCoCrFeNi

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Abstract

In this paper, the results of study of the AlCoCrFeNi high-entropy alloy by means of atom probe tomography are presented. Two phases were found, one enriched in Fe and Cr and the other enriched in Ni and Al. Owing to the complex surface morphology and spatial configuration of the phases, they were analyzed by various statistical methods. The Fe–Cr phase has a honeycomb structure that contains Co particles with the characteristic size of ~10 nm. The enrichment of the cell boundaries in Fe and Cr atoms reaches 50 at %. In turn, the Al–Ni phase is enriched in each of these elements up to 30 at % and contains nanoscale precipitates of Fe and Cr atoms. The volume density of these clusters is ~5 × 1022 cm–3.

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REFERENCES

  1. J.-W. Yeh, S.-K. Chen, S.-J. Lin, J.-Y. Gan, T.-S. Chin, T.-T. Shun, C.-H. Tsau, and S.-Y. Chang, Adv. Eng. Mater. 6, 299 (2004).

    Article  Google Scholar 

  2. B. Cantor, I. T. H. Chang, P. Knight, and A. J. B. Vincent, Mater. Sci. Eng. A 375–377 (2004).

  3. J.-W. Yeh, J. Miner. Met. Mater. Soc. 67, 2254 (2015).

    Article  Google Scholar 

  4. K.-Y. Tsai, M.-H. Tsai, and J.-W. Yeh, Acta Mater. 61, 4887 (2013).

    Article  ADS  Google Scholar 

  5. T. Egami, W. Guo, P. D. Rack, and T. Nagase, Metall. Mater. Trans. A 45, 180 (2014).

    Article  Google Scholar 

  6. S. J. Zinkle and L. L. Snead, Ann. Rev. Mater. Res. 44, 241 (2014).

    Article  ADS  Google Scholar 

  7. G. A. Salishchev, M. A. Tikhonovsky, D. G. Shaysultanov, N. D. Stepanov, A. V. Kuznetsov, I. V. Kolodiy, A. S. Tortika, and O. N. Senkov, J. Alloys Compd. 591, 11 (2014).

    Article  Google Scholar 

  8. A. Gali and E. P. George, Intermetallics 39, 74 (2013).

    Article  Google Scholar 

  9. M. Kang, J. W. Won, J. B. Kwon, and Y. S. Na, Mater. Sci. Eng. A 707, 16 (2017).

    Article  Google Scholar 

  10. B. Gludovatz, A. Hohenwarter, D. Catoor, E. H. Chang, E. P. George, and R. O. Ritchie, Science (Washington, DC, U. S.) 345 (6201), 1153 (2014).

    Article  ADS  Google Scholar 

  11. M. A. Hemphill, T. Yuan, G. Y. Wang, J. W. Yeh, C. W. Tsai, A. Chuang, and P. K. Liaw, Acta Mater. 60, 5723 (2012).

    Article  ADS  Google Scholar 

  12. M.-H. Chuang, M. H. Tsai, W.-R. Wang, S.-J. Lin, and J.-W. Yeh, Acta Mater. 59, 6308 (2011).

    Article  ADS  Google Scholar 

  13. C. J. Tong, M. R. Chen, S. K. Chen, J. W. Yeh, T. T. Shun, S. J. Lin, and S. Y. Chang, Metall. Mater. Trans. A 36A, 1263 (2005).

    Article  ADS  Google Scholar 

  14. J. W. Yeh, Y. L. Chen, S. J. Lin, and S. K. Chen, in Advanced Structural Materials, Ed. by H. B. Ramirez, J. G. Cabanas-Moreno, H. A. Calderon-Benavides, K. Ishizaki, and A. Salinas Rodriguez (2007), Vol. 3, p. 1.

    Google Scholar 

  15. S. Singh, N. Wanderka, B. S. Murty, and U. Glatze, Intermetallics 59, 182 (2011).

    Google Scholar 

  16. C. M. Lin and H. L. Tsai, Intermetallics 19, 288 (2011).

    Article  Google Scholar 

  17. T. T. Shun and Y. C. Du, J. Alloys Compd. 479, 157 (2009).

    Article  Google Scholar 

  18. Y. P. Wang, B. S. Li, M. X. Ren, C. Yang, and H. Z. Fu, Mater. Sci. Eng. A 491, 154 (2008).

    Article  Google Scholar 

  19. T. T. Shun, C. H. Hung, and C. F. Lee, J. Alloys Compd. 495, 55 (2010).

    Article  Google Scholar 

  20. Y. Linden, M. Pinkas, A. Munitz, and L. Meshi, Scr. Mater. 139, 49 (2017).

    Article  Google Scholar 

  21. S. V. Rogozhkin, A. A. Aleev, A. A. Lukyanchuk, A. S. Shutov, O. A. Raznitsyn, and S. E. Kirillov, Instrum. Exp. Tech. 60, 428 (2017).

    Article  Google Scholar 

  22. A. A. Aleev, S. V. Rogozhkin, A. A. Luk’yanchuk, A. S. Shutov, O. A. Raznitsyn, A. A. Nikitin, N. A. Iskandarov, O. A. Korchuganova, and S. E. Kirillov, State Registration Certificate of Computer Program No. 2018661876 (2018).

  23. O. A. Raznitsyn, A. A. Lukyanchuk, A. S. Shutov, S. V. Rogozhkin, and A. A. Aleev, J. Anal. Chem. 72, 1404 (2017).

    Article  Google Scholar 

  24. M. K. Miller, Atom Probe Tomography: Analysis at the Atomic Level (Kluwer Academic, New York, 2000).

    Book  Google Scholar 

  25. T. J. Godfrey, M. G. Hetherington, J. M. Sassen, and G. D. W. Smith, J. Phys. (Paris) 49 (C6), 421 (1988).

    Article  Google Scholar 

  26. J. M. Hyde, A. Cerezo, and T. J. Williams, Ultramicroscopy 109, 502 (2009).

    Article  Google Scholar 

  27. B. Gault and M. P. Moody, Springer Ser. Mater. Sci. 160, 240 (2012).

    Google Scholar 

  28. W. E. Lorensen and H. E. Cline, Comput. Graphics 21, 163 (1987).

    Article  Google Scholar 

  29. B. Gault and M. P. Moody, Springer Ser. Mater. Sci. 160, 233 (2012).

    Google Scholar 

  30. V. A. Epanechnikov, Theory Prob. Appl. J. 14, 153 (1969).

    Article  MathSciNet  Google Scholar 

  31. M. K. Miller and E. A. Kenik, Microsc. Microanal. 10, 336 (2004).

    Article  ADS  Google Scholar 

  32. M. K. Miller, J. M. Hyde, M. G. Hetherington, A. Cerezo, G. D. W. Smith, and C. M. Elliott, Acta Metall. Mater. 43, 3385 (1995).

    Article  Google Scholar 

  33. A. Manzoni, H. Daoud, R. Völkl, U. Glatzel, and N. Wanderka, Ultramicroscopy 132, 212 (2013).

    Article  Google Scholar 

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Funding

This work was supported by the Russian Foundation for Basic Research, project no. 18-38-00859. The atom probe tomography examinations were performed at the KAMIKS Shared Access Center (http://kamiks.itep.ru/) at the Alikhanov Institute for Theoretical and Experimental Physics, National Research Center “Kurchatov Institute.”

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Correspondence to A. S. Shutov.

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Translated by N. Semenova

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Rogozhkin, S.V., Shutov, A.S., Khomich, A.A. et al. Atom Probe Tomography of High-Entropy Alloy AlCoCrFeNi. Phys. Atom. Nuclei 83, 1644–1655 (2020). https://doi.org/10.1134/S106377882010021X

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