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Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl]benzamide : N,N-dimethylformamide (1 : 1)

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Abstract

The title compound, 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl] benzamide:N,N-dimethylformamide (1: 1), (C15H11N3O2S2 · C3H7NO), was synthesized, and its structure was established by spectral analysis and X-ray diffraction studies. The compound crystallizes in the monoclinic space group P21/n with a = 10.8714(7), b = 9.0497(5), c = 19.8347(13) Å, β = 91.093(5)°, Z = 4. The crystal structure is stabilized by N–H···S, C–H···O and N–H···O hydrogen bonds. The π···π interactions are also observed between the rings.

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Authors and Affiliations

  1. X-ray Crystallography Laboratory, Department of Physics, University of Jammu, Tawi, India

    P. Sharma & R. Kant

  2. Department of Chemistry, Mangalore University, Mangalagangotri, D.K., India

    K. N. Subbulakshmi & B. Narayana

  3. Industrial Chemistry Division, Department of Studies in Chemistry, Mangalore University, Mangalagangothri, D.K., India

    B. K. Sarojini

Authors
  1. P. Sharma
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  2. K. N. Subbulakshmi
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  3. B. Narayana
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  4. B. K. Sarojini
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  5. R. Kant
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Correspondence to R. Kant.

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Sharma, P., Subbulakshmi, K.N., Narayana, B. et al. Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl]benzamide : N,N-dimethylformamide (1 : 1). Crystallogr. Rep. 61, 230–233 (2016). https://doi.org/10.1134/S106377451602022X

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  • DOI: https://doi.org/10.1134/S106377451602022X

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