Abstract
The title compound, 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl was synthesized from 1-choloro-2.5-dimethoxy benzene, 1,3,5-triisopropylbenzene boronic acid and potassium phosphate in the presence of lead acetate as a catalyst and toluene as a solvent. Its crystal structure is determined by X-ray structure analysis. The crystals are the orthorhombic, a = 12.3281(4), b = 17.4235(5), c = 19.6550(6) Å, Z = 8, sp. gr. Pbca. R = 0.0603 for 2494 observed reflections.
Similar content being viewed by others
References
D. J. Cram, Angew. Chem. 100, 1041 (1988a).
D. J. Cram, Angew. Chem. Int. Ed. 27, 1009 (1988b).
N. A. Colabufo, F. Berardi, M. Cantore, et al., Bioorg. Med. Chem. 16, 3732 (2008).
P. Sharma, S. Chhabra, N. Rai, and N. Ghoshal, J. Chem. Inf. Model. 47, 1087 (2007).
B. S. Rathi, N. K. Wagh, S. L. Bodhankar, and V. M. Kulkarni, Arzneimittelforschung 56, 640 (2006).
M. Artico, A. Mai, G. Sbardella, et al., Bioorg. Med. Chem. Lett. 8, 1493 (1998)
B. A. Kimberly, S. Donna, A. C. Jon, et al., Epidemiology 21, 172 (2010).
M. Guoa, F. Jianb, and R. Hea, J. Fluorine Chem. 127, 177 (2006).
Oxford Diffraction (2010). CrysAlis PRO (Oxford Diffraction, Yarnton, England, 2010).
G. M. Sheldrick, Acta Crystallogr. A 64, 112 (2008).
L. J. Farrugia, J. Appl. Crystallogr. 45, 849 (2012).
M. Lahtinen, K. Nättinen, and S. Nummelin, Acta Crystallogr. E 69, o510 (2013).
F. H. Allen, O. Kennard, D. G. Watson, et al., J. Chem. Soc. Perkin Trans. 2, S1–19 (1987).
H. M. Seip and R. Seip, Acta Chem. Scand. 27, 4024 (1973).
G. Ferguson, C. Glidewell, and I. L. J. Patterson, Acta Crystallogr. C 52, 420 (1996).
I. L. J. Patterson, C. Glidewell, and G. Ferguson, Acta Crystallogr. C 54, 1970 (1998).
R. Abonia, C. Glidewell, J. N. Low, et al., Acta Crystallogr. C 59, o237 (2003).
J. N. Low, J. Cobo, J. Portilla, et al., Acta Crystallogr. E 60, o1034 (2004).
A. L. Spek, Acta Crystallogr. D 65, 148 (2009).
M. Nardelli, J. Appl. Crystallogr. 28, 659 (1995).
Author information
Authors and Affiliations
Corresponding author
Additional information
The article is published in the original.
Rights and permissions
About this article
Cite this article
Sharma, N., Prashanth, T., Lakshmi Ranganatha, V. et al. Crystal structure of 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl. Crystallogr. Rep. 60, 1116–1120 (2015). https://doi.org/10.1134/S1063774515070214
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1063774515070214