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Crystal structure of 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl

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Abstract

The title compound, 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl was synthesized from 1-choloro-2.5-dimethoxy benzene, 1,3,5-triisopropylbenzene boronic acid and potassium phosphate in the presence of lead acetate as a catalyst and toluene as a solvent. Its crystal structure is determined by X-ray structure analysis. The crystals are the orthorhombic, a = 12.3281(4), b = 17.4235(5), c = 19.6550(6) Å, Z = 8, sp. gr. Pbca. R = 0.0603 for 2494 observed reflections.

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References

  1. D. J. Cram, Angew. Chem. 100, 1041 (1988a).

  2. D. J. Cram, Angew. Chem. Int. Ed. 27, 1009 (1988b).

  3. N. A. Colabufo, F. Berardi, M. Cantore, et al., Bioorg. Med. Chem. 16, 3732 (2008).

    Article  Google Scholar 

  4. P. Sharma, S. Chhabra, N. Rai, and N. Ghoshal, J. Chem. Inf. Model. 47, 1087 (2007).

    Article  Google Scholar 

  5. B. S. Rathi, N. K. Wagh, S. L. Bodhankar, and V. M. Kulkarni, Arzneimittelforschung 56, 640 (2006).

    Google Scholar 

  6. M. Artico, A. Mai, G. Sbardella, et al., Bioorg. Med. Chem. Lett. 8, 1493 (1998)

    Article  Google Scholar 

  7. B. A. Kimberly, S. Donna, A. C. Jon, et al., Epidemiology 21, 172 (2010).

    Article  Google Scholar 

  8. M. Guoa, F. Jianb, and R. Hea, J. Fluorine Chem. 127, 177 (2006).

    Article  Google Scholar 

  9. Oxford Diffraction (2010). CrysAlis PRO (Oxford Diffraction, Yarnton, England, 2010).

    Google Scholar 

  10. G. M. Sheldrick, Acta Crystallogr. A 64, 112 (2008).

    Article  ADS  Google Scholar 

  11. L. J. Farrugia, J. Appl. Crystallogr. 45, 849 (2012).

    Article  Google Scholar 

  12. M. Lahtinen, K. Nättinen, and S. Nummelin, Acta Crystallogr. E 69, o510 (2013).

    Article  Google Scholar 

  13. F. H. Allen, O. Kennard, D. G. Watson, et al., J. Chem. Soc. Perkin Trans. 2, S1–19 (1987).

    Article  Google Scholar 

  14. H. M. Seip and R. Seip, Acta Chem. Scand. 27, 4024 (1973).

    Article  Google Scholar 

  15. G. Ferguson, C. Glidewell, and I. L. J. Patterson, Acta Crystallogr. C 52, 420 (1996).

    Article  Google Scholar 

  16. I. L. J. Patterson, C. Glidewell, and G. Ferguson, Acta Crystallogr. C 54, 1970 (1998).

    Article  Google Scholar 

  17. R. Abonia, C. Glidewell, J. N. Low, et al., Acta Crystallogr. C 59, o237 (2003).

    Article  Google Scholar 

  18. J. N. Low, J. Cobo, J. Portilla, et al., Acta Crystallogr. E 60, o1034 (2004).

    Article  Google Scholar 

  19. A. L. Spek, Acta Crystallogr. D 65, 148 (2009).

    Article  Google Scholar 

  20. M. Nardelli, J. Appl. Crystallogr. 28, 659 (1995).

    Article  Google Scholar 

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Correspondence to V. K. Gupta.

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Sharma, N., Prashanth, T., Lakshmi Ranganatha, V. et al. Crystal structure of 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl. Crystallogr. Rep. 60, 1116–1120 (2015). https://doi.org/10.1134/S1063774515070214

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  • DOI: https://doi.org/10.1134/S1063774515070214

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