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Crystal and molecular structure of (Z)-4-(((Z)-(2-oxonaphthalen-1(2H)-ylidene)methyl)amino)-N-(thiazol-2(3H)-ylidene)benzenesulfonamide

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Abstract

The experimental geometry of the title compound, (Z)-4-(((Z)-(2-oxonaphthalen-1(2H)-ylidene)methyl)amino)-N-(thiazol-2(3H)-ylidene)benzene, C20H15N3O3S2, was characterized by X-ray diffraction analysis (XRD). And also SEM analysis has been done for morphological investigation of the crystal structure. Molecular structure crystallizes in triclinic form, space group P \(\overline 1\) with a = 9.1398(7), b = 10.1524(7), c = 11.3767(8) Å, α = 114.488°, β = 91.380(6)°, γ = 102.006(6)° and V = 932.44(12) Å3. In the solid state of the molecular structure C–H···O and N–H···O type interactions provide for stabilization.

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References

  1. H. Chen and J. Rhodes, J. Mol. Med. 74, 497 (1996).

    Article  Google Scholar 

  2. S. Uhlenbrock, R. Wegner, and B. Krebs, J. Chem. Soc. Dalton Trans. 3731 (1996).

    Google Scholar 

  3. O. P. Anderson, A. la Cour, M. Findeisen, et al., J. Chem. Soc. Dalton Trans. 111. (1997).

    Google Scholar 

  4. M. Singh, Curr. Pharm. Des. 5, 443 (1999).

    Google Scholar 

  5. V. Ambike, S. Adsule, F. Ahmed, et al., J. Inorg. Biochem. 101, 1517 (2007).

    Article  Google Scholar 

  6. A. Vijayaraj, R. Prabu, R. Suresh, N. Mathivanan, and V. Narayanan, Synth. React. Inorg., Met.-Org., Nano-Met. Chem. 45, 1647 (2015).

    Article  Google Scholar 

  7. Stoe & Cie. X-AREA (Version 1.18) and X-RED32 (Version 1.04) (Stoe & Cie, Darmstadt, Germany, 2002).

  8. G. M. Sheldrick, SADABS (Univ. of Göttingen, Göttingen, Germany, 1996).

    Google Scholar 

  9. G. M. Sheldrick, Acta Crystallogr. A 64, 112 (2008).

    Article  ADS  Google Scholar 

  10. L. J. Farrugia, J. Appl. Crystallogr. 30, 565 (1997).

    Article  Google Scholar 

  11. L. J. Farrugia, J. Appl. Crystallogr. 32, 837 (1999).

    Article  Google Scholar 

  12. K. Amimoto and T. J. Kawato, Photochem. Photobiol. C 6, 207 (2005).

    Article  Google Scholar 

  13. G. M. J. Schmidt and M. D. Cohen, J. Chem. Soc. 1996 (1964).

    Google Scholar 

  14. E. Temel, E. Agar, and O. Büyükgüngör, Acta Crystallogr. E 66, o1131 (2010).

    Article  Google Scholar 

  15. S. Ibrahim, M. N. Tahir, N. Iqbal, et al., Acta Crystallogr. E 67, o298 (2011).

    Article  Google Scholar 

  16. J. Bernstein, R. E. Davis, L. Shimoni, and N.-L. Chang, Angew. Chem. Int. Ed. Engl. 34, 1555 (1995).

    Article  Google Scholar 

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Authors and Affiliations

  1. Yeşilyurt Demir-Çelik Vocational School, Ondokuz Mayıs University, Samsun, Turkey

    Y. Köysal

  2. Department of Physics, Faculty of Arts and Sciences, Ondokuz Mayıs University, Samsun, Turkey

    H. Bülbül & N. Dege

  3. Department of Chemistry, Faculty of Arts and Sciences, Ondokuz Mayıs University, Samsun, Turkey

    M. Macit & A. Alaman Ağar

Authors
  1. Y. Köysal
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  2. H. Bülbül
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  3. N. Dege
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  4. M. Macit
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  5. A. Alaman Ağar
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Correspondence to Y. Köysal.

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Köysal, Y., Bülbül, H., Dege, N. et al. Crystal and molecular structure of (Z)-4-(((Z)-(2-oxonaphthalen-1(2H)-ylidene)methyl)amino)-N-(thiazol-2(3H)-ylidene)benzenesulfonamide. Crystallogr. Rep. 60, 1001–1005 (2015). https://doi.org/10.1134/S1063774515070147

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  • DOI: https://doi.org/10.1134/S1063774515070147

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