Skip to main content
Log in

Growth and analysis of NSH and KMNSH crystals by slow evaporation technique

  • Crystal Growth
  • Published:
Crystallography Reports Aims and scope Submit manuscript

Abstract

Nickel Sulphate Hexahydrate (NSH) and Potassium Magnesium Nickel Sulphate Hexahydrate (KMNSH) single crystals were grown by slow evaporation method. The grown NSH crystal was found to crystallize in tetragonal system with space group P41212 and KMNSH in monoclinic system with space group P 121/c. The optical band gap energies of the grown crystals using UV-Vis spectral results for the doped and undoped NSH crystals were calculated. The presence of various functional groups in the crystal was identified by FTIR analysis. The thermal behaviour of the grown crystal has been studied by TGA/DTA analysis.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. N. B. Singh and W. D. Partlow, U.S. Patent No. 5788765 (1998).

  2. H. Youping, C. Jianrong, S. Genbo, et al., J. Cryst. Growth. 233, 809 (2001).

    Article  Google Scholar 

  3. E. B. Rudneva, V. L. Mamomenova, L. F. Malakhova, et al., Crystallogr. Rep. 51, 344 (2006).

    Article  ADS  Google Scholar 

  4. G. Su, X. Zhuang, Y. He, Zh. Li, et al., J. Cryst. Growth. 243, 238 (2002).

    Article  ADS  Google Scholar 

  5. X. Wang, X. Zhuang, G. Su, and Y. He, Opt. Mater. 31, 233 (2008).

    Article  ADS  Google Scholar 

  6. G. Su, X. Zhuang, Y. He, and G. Zheng, Opt. Mater. 30, 916 (2008).

    Article  ADS  Google Scholar 

  7. S. Radhika, C. M. Padma, S. Ramalingom, and T. Chithambara Thanu, Arch. Phys. Res. 4, 49 (2013).

    Google Scholar 

  8. S. Bin Anooz, R. Bertramb, and D. Klimm, Solid State Commun. 141, 497 (2007)

    Article  ADS  Google Scholar 

  9. X. X. Zhang, G. B. Su, Y. P. He, and G. Z. Zheng, Cryst. Res. Tech. 41, 1031 (2006).

    Article  Google Scholar 

  10. I. Polovynko, S. Rykhlyuk, I. Karbovnyk, et al., J. Cryst Growth. 311, 4704 (2009).

    Article  ADS  Google Scholar 

  11. V. Krishnakumar, C. Ramachandraraja, and R. S. Sundararajan, Spectrochim. Acta A 68, 113 (2007).

    Article  ADS  Google Scholar 

  12. S. Karan and S. P. Sen Gupta, Mater. Sci. Eng. 398, 198 (2005).

    Article  Google Scholar 

  13. D. Vanitha, S. Asath Bahadur, and Athimoolam, Arc. Appl. Sci. Res. 4, 2378 (2012).

    Google Scholar 

  14. A. Ruby and A. Cecil Raj, Arch. Phys. Res. 3, 130 (2012).

    Google Scholar 

  15. G. Sivanesan, P. Kolandaivel, and S. Selvasekarapaandian, Mat. Chem. Phys. 34, 73 (1993).

    Article  Google Scholar 

  16. Y. He, J. Chen, G. Su, et al., J. Cryst. Growth. 233, 809 (2001).

    Article  ADS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to J. Shanthi.

Additional information

The article is published in the original.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Masilamani, V., Shanthi, J. & Sheelarani, V. Growth and analysis of NSH and KMNSH crystals by slow evaporation technique. Crystallogr. Rep. 59, 1114–1117 (2014). https://doi.org/10.1134/S1063774514070141

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1063774514070141

Keywords

Navigation