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Structure analysis of O,O’-propane-1,3-diyl bis[diphenyl(phosphinothioate)]

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Abstract

A new diphosphine disulphide compound with the formula C27H26O2|P2S2, was synthesized from the reaction between PPh2SCl and 1,3-propanediol and characterized with different spectroscopic methods. Its structure has also been studied by X-ray diffraction. The compound crystallizes in the triclinic space group \(P\bar 1\). Pentavalent phosphorus atoms in the molecule are in distorted tetrahedral environments.

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Authors and Affiliations

  1. Faculty of Science, Chemistry Department, Ege University, 35100, Izmir, Turkey

    M. Karaman & S. Irisli

  2. Faculty of Science and Literature, Physics Department, Ondokuz Mayıs University, 55139, Samsun, Turkey

    O. Büyükgüngör

Authors
  1. M. Karaman
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  2. S. Irisli
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  3. O. Büyükgüngör
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Correspondence to S. Irisli.

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Karaman, M., Irisli, S. & Büyükgüngör, O. Structure analysis of O,O’-propane-1,3-diyl bis[diphenyl(phosphinothioate)]. Crystallogr. Rep. 58, 1088–1090 (2013). https://doi.org/10.1134/S1063774513080051

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  • DOI: https://doi.org/10.1134/S1063774513080051

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