Abstract
The electric and structural characteristics of silicon-doped GaN and Al0.3Ga0.7N layers grown by molecular beam epitaxy (MBE) using silane have been analyzed by the Hall effect, Raman spectroscopy, and high-resolution X-ray diffractometry. It is established that the electron concentration linearly increases up to n = 4 × 1020 cm−3 with an increase in the silane flow rate for GaN:Si, whereas the corresponding dependence for Al0.3Ga0.7N:Si is sublinear and the maximum electron concentration is found to be n = 4 × 1019 cm−3. X-ray measurements of sample macrobending indicate a decrease in biaxial compressive stress with an increase in the electron concentration in both GaN:Si and Al0.3Ga0.7N:Si layers. The parameters of the dislocation structure, estimated from the measured broadenings of X-ray reflections, are analyzed.
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N. M. Shmidt, A. V. Lebedev, W. V. Lundin, et al., Mater. Sci. Eng., B59, 195 (1999).
A. Cremades, L. Gorgens, O. Ambacher, et al., Phys. Rev. B 61, 2812 (2000).
L. T. Romano, C. G. van de Walle, J. W. Ager III, et al., J. Appl. Phys. 87, 7745 (2000).
T. Bottcher, S. Einfeldt, R. Figge, et al., Appl. Phys. Lett. 78, 1976 (2001).
P. Cantu, F. Wu, Waltereit, et al., Appl. Phys. Lett. 83, 674 (2003).
D. Follstaed, S. R. Lee, Allerman, et al., J. Appl. Phys. 105, 083507 (2009).
I. Manning, X. Weng, J. D. Acord, et al., J. Appl. Phys. 106, 023506 (2009).
J. Xie, S. Mita, A. Rice, et al., Appl. Phys. Lett. 98, 202101 (2011).
F. Brunner, A. Mogilatenko, A. Knauer, et al., J. Appl. Phys. 112, 033503 (2012).
M. A. Moram, M. J. Kappers, F. Massabuau, et al., 109, 073509.
K. Forghani, L. Schde, U. T. Schwarz, et al., J. Appl. Phys. 112, 093102 (2012).
G. A. Rozgonii and T. J. Ciesielka, Rev. Sci. Instrum. 44, 1053 (1973).
P. Y. Fewster and A. Andrew, J. Appl. Crystallogr. 20, 451 (1995).
M. V. Klein, B. N. Ganguly, and P. J. Colwell, Phys. Rev. B 6, 2380 (1972).
V. V. Emtsev, V. Yu. Davydov, V. V. Kozlovskii, et al., Semicond. Sci. Technol. 15, 73 (2000).
V. Yu. Davydov, N. S. Averkiev, I. N. Goncharuk, et al., J. Appl. Phys. 82, 5097 (1997).
G. G. Stoney, Proc. R. Soc. London, Ser. A 82, 172 (1909).
A. F. Wright, J. Appl. Phys. 82, 2833 (1997).
I. Vurgaftman and J. R. Meyer, J. Appl. Phys. 94, 3675 (2003).
Landolt-Bornstein, Ed. by O. Madelung (Springer, New York, 1982), Vol. 17.
J. G. Kim, A. Kimura, Y. Kamei, et al., J. Appl. Phys. 110, 033511 (2011).
V. V. Ratnikov, R. N. Kyutt, T. V. Shubina, et al., J. Phys. D: Appl. Phys. 34, A30 (2001).
A. Y. Polyakov, N. B. Smirnov, A. V. Govorkov, et al., Solid-State Electron. 42, 627 (1998).
B. Borisov, V. Kuryatkov, Yu. Kudryavtsev, et al., Appl. Phys. Lett. 87, 132106 (2005).
S. Heanre, E. Chason, J. Han, et al., Appl. Phys. Lett. 74, 356 (1999).
Z. Chine, A. Rebey, H. Touati, et al., Phys. Status Solidi A 203, 1954 (2006).
V. Yu. Davydov, I. N. Goncharuk, A. N. Smirnov, et al., Phys. Rev. B 65, 125203 (2002).
X-O. Shen, S. Tanaka, S. Iwai, et al., Appl. Phys. Lett. 80, 2008 (1998).
S. Tanaka, M. Takeuchi, and Y. Aoyagi, Jpn. J. Appl. Phys. Part 2, 39, L831 (2000).
C. G. Dunn and E. F. Koch, Acta Metall. 5, 548 (1957).
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Ratnikov, V.V., Kyutt, R.N., Smirnov, A.N. et al. Defects and stresses in MBE-grown GaN and Al0.3Ga0.7N layers doped by silicon using silane. Crystallogr. Rep. 58, 1023–1029 (2013). https://doi.org/10.1134/S106377451307016X
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DOI: https://doi.org/10.1134/S106377451307016X