Skip to main content
SpringerLink
Log in

Synthesis and crystal structure of 3-ammoniumphenyl sulfone selenate, 3-aminophenyl sulfone [C12H14N2O2S]SeO4 · [C12H12N2O2S]

  • Structure of Organic Compounds
  • Published:
Crystallography Reports Aims and scope Submit manuscript

Abstract

The crystal structure of [C12H14N2O2S]SeO4 · [C12H12N2O2S] was determined by X-ray diffraction on single crystal. Crystals are orthorhombic, space group Pbca, with cell parameters a = 11.545 (1), b = 8.143 (1), c = 55.783(1)Å, V = 5244.2 (8)Å3 and Z = 8. The structure can be described as organic layers built by [C12H14N2O2S]2+ cations and [C12H12N2O2S] molecules, parallel to ab plane, between which the inorganic groups SeO 2−4 are inserted. In this atomic arrangement, H-bonds between the different species play an important role in the three-dimensional network cohesion.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Nonlinear Optical Properties of Organic Molecules and Crystals, Ed. by D. S. Chemla and J. Zyss (Academic, Orlando, 1987).

    Google Scholar 

  2. M. Marchewka, J. Janczak, S. Debrus, J. Baran and H. Ratajczak, Solid State Sci. 5, 643 (2003).

    Article  ADS  Google Scholar 

  3. S. Bhattacharya, P. Dastidar and T. G. N. Row, Chem. Mater. 6, 531 (1994).

    Article  Google Scholar 

  4. N. Blagden and K. R. Seddon, Cryst. Eng. 2, 9 (1999).

    Article  Google Scholar 

  5. T. Głowiak, S. Debrus, M. May, A. J. Barnes and H. Ratajczak, J. Mol. Struct. 596, 77 (2001).

    Article  Google Scholar 

  6. M. Belhouchet, M. Bahri, J. M. Savariault and T. Mhiri, Spectrochim. Acta A 61, 387 (2005).

    Article  ADS  Google Scholar 

  7. M. Belhouchet, J. M. Savariault, and T. Mhiri, J. Phys. Chem. Solids 66, 1294 (2005).

    Article  ADS  Google Scholar 

  8. A. Mahroug, M. Belhouchet, A. Hémon-Ribaud and T. Mhiri, Phosphorus, Sulfur, and Silicon 186, 2332 (2011).

    Article  Google Scholar 

  9. G. M. Sheldrick, SHELXS-97: The Program for the Crystal Structure Solution (Univ. of Göttingen, Göttingen, 1997).

    Google Scholar 

  10. G. M. Sheldrick, SHELXL-97: Program for the Refinement of Crystal Structures (Univ. of Göttingen, Göttingen, 1997).

    Google Scholar 

  11. J. Janczak, G. Julio Perpétuo, Acta Crystallogr. C 65, o121 (2009).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Laboratoire Physico-Chimie de l’Etat Solide. Département de Chimie. Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisia

    A. Mahroug, M. Belhouchet & T. Mhiri

Authors
  1. A. Mahroug
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. Belhouchet
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. T. Mhiri
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to M. Belhouchet.

Additional information

The article is published in the original.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Mahroug, A., Belhouchet, M. & Mhiri, T. Synthesis and crystal structure of 3-ammoniumphenyl sulfone selenate, 3-aminophenyl sulfone [C12H14N2O2S]SeO4 · [C12H12N2O2S]. Crystallogr. Rep. 58, 613–616 (2013). https://doi.org/10.1134/S1063774513040263

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1063774513040263

Keywords

Search

Navigation