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Spectroscopic studies and crystal structure of (E)-N′-(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide

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Abstract

The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P21/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) Å, β = 110.42(1)°, V = 1270.7(3) Å3, D x = 1.418 g cm−3, R 1 = 0.0349 and wR 2 = 0.0935 [I > 2σ(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, 1H NMR, 13C NMR and UV-Visible spectroscopic techniques.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science and Arts, Çanakkaale Onsekiz Mart University, TR-17100, Çanakkaale, Turkey

    H. Ozay & M. Yildiz

  2. Nanoscience and Technology Research and Application Center (NANORAC), Çanakkale Onsekiz Mart University, TR-17100, Çanakkale, Turkey

    M. Yildiz

  3. Department of Physics, Faculty of Science, Ankara University, TR-06100, Tandoğan, Ankara, Turkey

    H. Unver

  4. Ataturk Faculty of Education, Near East University, Nicosia, Mersin 10, Turkey

    A. Kiraz

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  1. H. Ozay
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  2. M. Yildiz
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  3. H. Unver
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  4. A. Kiraz
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Correspondence to H. Ozay.

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Ozay, H., Yildiz, M., Unver, H. et al. Spectroscopic studies and crystal structure of (E)-N′-(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide. Crystallogr. Rep. 58, 106–110 (2013). https://doi.org/10.1134/S1063774513010264

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  • DOI: https://doi.org/10.1134/S1063774513010264

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