Abstract
We discuss an ion-optical system (IOS) of a mass spectrometer designed for isotopic measurements of light gases, containing a magnetic prism with plane-parallel pole tips and two sector-wise, cylindrical-capacitor identical in geometry, symmetrically located relative to the prism. The relationships between the geometric parameters of the capacitors and the prism are given, which are necessary to ensure achromatic focusing of the ion beam in the plane of the detector receiving slit. We assessed numerically the effect of IOS aberrations on the mass resolution of the IOS and determined the optimal emittance of the ion beam at the source output, which enables achieving a resolution at the level of 3000–3500 with an output slit of the ion source of approximately 50 μm, high transmittance of the mass analyzer, small dimensions of the magnetic prism, and a moderate total length of the central ion trajectory (less than 1 m). The IOS is characterized by a high dispersion in masses, which is much larger than the dispersion of conventional sector magnetic mass spectrometers of the same dimensions. The IOS consists of simple geometry elements, which reduces the costs of its implementation and makes the mass spectrometer technologically advanced and convenient to set up and operate.
Similar content being viewed by others
REFERENCES
Gall’, L.N., Semenov, A.A., Kudriavtsev, V.N., et al., Nauchn, Priborostr., 2016, vol. 26, no. 3, p. 24.
Mazhejka, I., Pyatroshyus, R., Yasyulenis, R., et al., At. Energ., 1993, vol. 75, no. 6, p. 471.
Ratia, G.G. and Bonchuk, Y.V., Radiat. Gig., 2009, vol. 2, no. 2, p. 48.
Gross, J.H., Mass Spectrometry, Berlin: Springer, 2011.
Kel’man, V.M. and Gall’, L.N., Zh. Tekh. Fiz., 1961, vol. 31, no. 9, p. 1083.
Gall’, R.N., Gall’, L.N., Kel’man, V.M., et al., USSR Patent 353186, 1972.
Kel’man, V.M., Karetskaya, S.P., Fedulina, L.V., et al., Elektronno-opticheskie elementy prizmennykh spektrometrov zaryazhennykh chastits (Electron-Optical Elements of Prism Charged Particle Spectrometers), Alma-Ata: Nauka, 1979.
Kel’man, V.M., Nazarenko, L.M., and Yakushev, E.M., Zh. Tekh. Fiz., 1972, vol. 42, p. 963.
Bimurzaev, S.B., Voronin, B.M., Kel’man, V.M., et al., Zh. Tekh. Fiz., 1983, vol. 53, p. 2195.
Kel’man, V.M. and Yavor, S.Ya., Elektronnaya optika (Electron Optics), Leningrad: Nauka, 1968, 3rd ed.
Yavor, M.I. and Berdnikov, A.S., Nucl. Instrum. Methods Phys. Res., Sect. A, 1995, vol. 363, nos. 1–2, p. 416.
Berz, M., Nucl. Instrum. Methods Phys. Res., Sect. A, 1990, vol. 298, p. 473.
Cosy Infinity. http://www.bt.pa.msu.edu/index_cosy.html.
Brown, K.L. and Spencer, J.E., IEEE Trans. Nucl. Sci., 1981, vol. 28, no. 3, p. 2568.
Funding
This work was partially supported by the State Assignment to the Institute for Analytical Instrumentation, Russian Academy of Sciences, project no. 075-00780-19-00.
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated by O. Zhukova
Rights and permissions
About this article
Cite this article
Sachenko, V.D., Yakushev, E.M., Nazarenko, L.M. et al. An Ion-Optical Circuit of a Small-Sized Mass-Spectrometer for the Isotope Analysis of Hydrogen–Helium Mixtures. J Anal Chem 75, 1693–1699 (2020). https://doi.org/10.1134/S1061934820130134
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1061934820130134