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Journal of Analytical Chemistry

, Volume 72, Issue 14, pp 1404–1410 | Cite as

Optimization of Material Analysis Conditions for Laser-Assisted Atom Probe Tomography Characterization

  • O. A. RaznitsynEmail author
  • A. A. Lukyanchuk
  • A. S. Shutov
  • S. V. Rogozhkin
  • A. A. Aleev
Articles

Abstract

Atom probe tomography (APT) analysis with a femtosecond laser is one of the most promising techniques to characterize local variations of chemical distribution in materials with subnanometer spatial resolution. In this study, the effect of APT analysis conditions on the accuracy of data recovery for chromium steels and Fe-Cr alloys is investigated. Dependences of mass resolving power and the detected composition of chromium as a function of laser power, specimen geometry, and evaporation rate are presented.

Keywords

atom probe tomography time-of-flight mass spectrometer laser evaporation 

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References

  1. 1.
    Tolstoguzov, A.B., Mass-Spektrom., 2009, vol. 6, no. 4, p. 280.Google Scholar
  2. 2.
    Rogozhkin, S.V., Aleev, A.A., Lukyanchuk, A.A., Shutov, A.S., Raznitsyn, O.A., and Kirillov, S.E., Instrum. Exp. Tech., 2017, vol. 60, no. 3, p. 428.CrossRefGoogle Scholar
  3. 3.
    Kellogg, G.L. and Tsong, T.T., J. Appl. Phys., 1980, vol. 51, no. 2, p. 1184.CrossRefGoogle Scholar
  4. 4.
    Gault, B., Moody, M.P., Cairney, J.M., and Ringer, S.P., Atom Probe Microscopy, New York: Springer, 2012.CrossRefGoogle Scholar
  5. 5.
    Rogozhkin, S.V., Nikitin, A.A., Aleev, A.A., Germanov, A.B., and Zaluzhnyi, A.G., Inorg. Mater.: Appl. Res., 2013, vol. 4, no. 2, p. 112.CrossRefGoogle Scholar
  6. 6.
    Aleev, A.A., Iskandarov, N.A., Klimenkov, M., Lindau, R., Moslang, A., Nikitin, A.A., Rogozhkin, S.V., Vladimirov, P., and Zaluzhnyi, A.G., J. Nucl. Mater., 2011, vol. 409, no. 2, p. 65.CrossRefGoogle Scholar
  7. 7.
    Rogozhkin, S.V., Ageev, V.S., Aleev, A.A., Zaluzhnyi, A.G., Leont’eva-Smirnova, M.V., and Nikitin, A.A., Phys. Met. Metallogr., 2009, vol. 108, no. 6, p. 579.CrossRefGoogle Scholar
  8. 8.
    Rogozhkin, S.V., Bogachev, A. A., Kirillov, D. I., Nikitin, A.A., Orlov, N.N., Aleev, A.A., Zaluzhnyi, A.G., and Kozodaev, M.A., Phys. Met. Metallogr., 2014, vol. 115, no. 12, p. 1259.CrossRefGoogle Scholar
  9. 9.
    Rogozhkin, S.V., Korchuganova, O.A., and Aleev, A.A., Inorg. Mater.: Appl. Res., 2016, vol. 7, no. 2, p. 210.CrossRefGoogle Scholar
  10. 10.
    Kelly, T.F., Vella, A., Bunton, J.H., Houard, J., Silaeva, E.P., Bogdanowicz, J., and Vandervorst, W., Curr. Opin. Solid State Mater., 2014, vol. 18, no. 2, p. 81.CrossRefGoogle Scholar
  11. 11.
    Houard, J., Vella, A., Vurpillot, F., and Deconihout, B., Phys. Rev. B: Condens. Matter Mater. Phys., 2010, vol. 81, nos. 1–5, 125411.CrossRefGoogle Scholar
  12. 12.
    Yiyou, Tu., Plotnikov, E.Y., and Seidman, D.N., Microsc. Microanal., 2015, vol. 21, no. 2, p. 480.CrossRefGoogle Scholar
  13. 13.
    Prakash Kollia, R. and Meisenkothen, F., Microsc. Microanal., 2014, vol. 20, no. 3, p. 768.CrossRefGoogle Scholar
  14. 14.
    Cerezo, A., Clifton, P.H., Gmberg, A., and Smith, G.D.W., Ultramicroscopy, 2007, vol. 107, no. 9, p. 720.CrossRefGoogle Scholar

Copyright information

© Pleiades Publishing, Ltd. 2017

Authors and Affiliations

  • O. A. Raznitsyn
    • 1
    • 2
    Email author
  • A. A. Lukyanchuk
    • 1
    • 2
  • A. S. Shutov
    • 1
    • 2
  • S. V. Rogozhkin
    • 1
    • 2
  • A. A. Aleev
    • 1
    • 2
  1. 1.Institute for Theoretical and Experimental Physics named by A.I. AlikhanovNational Research Centre “Kurchatov Institute”MoscowRussia
  2. 2.National Research Nuclear University MEPhI (Moscow Engineering Physics Institute)MoscowRussia

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