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Determination of individual sulfur-containing compounds in liquid hydrocarbon raw materials and their processing products by gas chromatography

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Abstract

The publications dedicated to the determination of individual sulfur-containing compounds in liquid hydrocarbon raw materials and their processing products by gas chromatography are summarized. In the analysis of petroleum raw materials, the preliminary separation of sulfur-containing compounds and a hydrocarbon matrix is usually performed. In the analysis of liquid oil refining products and gas condensate, the direct determination of individual sulfur-containing compounds can be frequently conducted. The use of currently available sulfur-selective chemiluminescence and atomic emission detectors in combination with nonpolar or slightly polar capillary columns and also two-dimensional chromatography is the most promising.

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References

  1. TR TS(Technical Regulations of the Customs Union) 013/2011: On Requirements to Automobile and Aviation Gasoline, Diesel and Marine Fuel, Jet Fuel, and Heating Oil, 2011.

  2. Novikov, E.A., Mir Nefteproduktov, 2008, no. 1, p. 28.

    Google Scholar 

  3. Novikov, E.A., Mir Nefteproduktov, 2008, no. 3, p. 27.

    Google Scholar 

  4. Nadkarni, R. and Kishore, A., Am. Lab., 2000, vol. 32, no. 1, p. 16.

    CAS  Google Scholar 

  5. Chertkov, Ya.B. and Spirkin, V.G., Sernistye i kislorodnye soedineniya neftyanykh distillyatov (Sulfur and Oxygen Compounds of Petroleum Distillates), Moscow Khimiya, 1971.

    Google Scholar 

  6. Obolentsev, R.D. and Baikova, A.Ya., Seraorganicheskie soedineniya neftei Uralo-Povolzh’ya i Sibiri (Organosulfur Compounds of Oils of Ural–Volga Region and Siberia), Moscow Nauka, 1973.

    Google Scholar 

  7. Bol’shakov, G.F., Seraorganicheskie soedineniya nefti (Organosulfur Compounds of Oil), Moscow Nauka, 1984.

    Google Scholar 

  8. Lyapina, N.K., Russ. Chem. Rev., 1982, vol. 51, no. 2, p. 189.

    Article  Google Scholar 

  9. Olufsen, B.S. and Bjorseth, A., in Handbook of Polycyclic Aromatic Hydrocarbons, Bjorseth, A., Ed., New York: Marcel Dekker, 1983, vol. 1, p. 257.

    Google Scholar 

  10. Schou, L. and Myhr, M.B., Org. Geochem., 1988, vol. 13, nos. 1–3, p. 61.

    Article  CAS  Google Scholar 

  11. Damste, J.S.S., Rijpstra, W.I.C., Leeuw, J.W., and Lijmbach, G.W.M., J. High Resolut. Chromatogr., 1994, vol. 17, no. 6, p. 489.

    Article  Google Scholar 

  12. Hegazi, A.H., Andersson, J.T., and El-Gayar, M.S., Fuel Process. Technol., 2003, vol. 85, no. 1, p. 1.

    Article  Google Scholar 

  13. Jacob, J., Sulfur Analogues of Polycyclic Aromatic Hydrocarbons (Thiaarenes), Cambridge Cambridge University Press, 1990.

    Google Scholar 

  14. Beens, J. and Tijssen, R., J. High Resolut. Chromatogr., 1997, vol. 20, no. 3, p. 131.

    Article  CAS  Google Scholar 

  15. Vassilaros, D.L., Kong, R.C., Later, D.W., and Lee,M.L., J. Chromatogr., 1982, vol. 252, no. 1, p. 1.

    Article  CAS  Google Scholar 

  16. Brazhnikov, V.V., Detektory dlya khromatografii (Detectors for Chromatography), Moscow Mashinostroenie, 1992.

    Google Scholar 

  17. Hua, R., Li, Y., Liu, W., Zheng, J., Wei, H., Wang, J., Lu, X., Kong, H., and Xu, G., J. Chromatogr. A, 2003, vol. 1019, nos. 1–2, p. 101.

    Article  CAS  Google Scholar 

  18. Hegazi, A.H. and Andersson, J.T., Energy Fuels, 2007, vol. 21, no. 6, p. 3375.

    Article  CAS  Google Scholar 

  19. Moustafa, N.E. and Andersson, J.T., Fuel Process. Technol., 2011, vol. 92, no. 3, p. 547.

    Article  CAS  Google Scholar 

  20. Song, Ch., Catal. Today, 2003, vol. 86, nos. 1–4, p. 211.

    Article  CAS  Google Scholar 

  21. Knudsen, K.G., Cooper, B.H., and Topsøe, H., Appl. Catal., A, 1999, vol. 189, no. 2, p. 205.

    Article  CAS  Google Scholar 

  22. Radchenko, E.D., Nefedov, B.G., and Aliev, R.R., Promyshlennye katalizatory gidrogenizatsionnykh protsessov neftepererabotki (Industrial Catalysts of Hydrogenation Refining Processes), Moscow Khimiya, 1987.

    Google Scholar 

  23. Topsøe, H., Clausen, B.S., and Massoth, F.E., in Catalysis: Science and Technology, Anderson, J.R. and Boudart, M., Eds., Berlin: Springer, 1996, vol. 11, p. 1.

    Google Scholar 

  24. Depauw, G.A. and Froment, G.F., J. Chromatogr. A, 1997, vol. 761, nos. 1–2, p. 231.

    Article  CAS  Google Scholar 

  25. Ruiz-Guerrero, R., Vendeuvre, C., Thiébaut, D., Bertoncini, F., and Espinat, D., J. Chromatogr. Sci., 2006, vol. 44, no. 9, p. 566.

    Article  CAS  Google Scholar 

  26. Bender, A.O., Sarkissian, T.M., and Allawi, A.M., Fuel, 1989, vol. 68, no. 5, p. 607.

    Article  CAS  Google Scholar 

  27. Andersson, J.T., J. Chromatogr. A, 1986, vol. 354, no. 1, p. 83.

    Article  CAS  Google Scholar 

  28. Andersson, J.T. and Schmid, B., J. Chromatogr. A, 1995, vol. 693, no. 2, p. 325.

    Article  CAS  Google Scholar 

  29. Hutte, R.S., in Chromatography in the Petroleum Industry, Adlard, E.R., Ed., Amsterdam: Elsevier, 1994, p. 201.

  30. Kong, R.C., Lee, M.L., Tominaga, Y., Pratap, R., Iwao, M., Castle, R.N., and Wise, S.A., J. Chromatogr. Sci., 1982, vol. 20, no. 11, p. 502.

    Article  CAS  Google Scholar 

  31. Nishioka, M., Jones, B.A., Tarbet, B.J., Bradshaw, J.S., and Lee, M.L., J. Chromatogr. A, 1986, vol. 357, no. 1, p. 79.

    Article  CAS  Google Scholar 

  32. Budzinski, H., Garrigues, P., and Bellocq, J., J. Chromatogr. A, 1992, vol. 590, no. 2, p. 297.

    Article  CAS  Google Scholar 

  33. Mössner, S.G., Lopez de Alda M.J., Sander, L.C., Lee, M.L., and Wise, S.A., J. Chromatogr. A, 1999, vol. 841, no. 2, p. 207.

    Article  Google Scholar 

  34. Becker, G. and Colmsjo, A., Anal. Chim. Acta, 1998, vol. 376, no. 3, p. 265.

    Article  CAS  Google Scholar 

  35. Mössner, S.G. and Wise, S.A., Anal. Chem., 1999, vol. 71, no. 1, p. 58.

    Article  Google Scholar 

  36. Lopez-Garcia, C., Becchi, M., Grenier-Loustalot, M.F., Paisse, O., and Szymansky, R., Anal. Chem., 2002, vol. 74, no. 15, p. 3849.

    Article  CAS  Google Scholar 

  37. Can, H., Dimoglo, A., and Kovalishyn, V., J. Mol. Struct.: THEOCHEM, 2005, vol. 723, nos. 1–3, p. 183.

    Article  CAS  Google Scholar 

  38. Safa, F. and Hadjmohammadi, M.R., QSAR Comb. Sci., 2005, vol. 24, no. 9, p. 1026.

    Article  CAS  Google Scholar 

  39. Schade, Th. and Andersson, J.T., J. Chromatogr. A, 2006, vol. 1117, no. 2, p. 206.

    Article  CAS  Google Scholar 

  40. Xua, H.-Y., Zoub, J.-W., Jiang, Y.-J., Hub, G.-X., and Yu, Q.-S., J. Chromatogr. A, 2008, vols. 1198–1199, no. 1, p. 202.

    Article  Google Scholar 

  41. Yin, C. and Xia, D., Fuel, 2004, vol. 83, nos. 4–5, p. 433.

    Article  CAS  Google Scholar 

  42. Chawla, B. and Di Sanzo, F.P., J. Chromatogr. A, 1992, vol. 589, nos. 1–2, p. 271.

    Article  CAS  Google Scholar 

  43. Quimby, B.D., Giarrocco, V., Sullivan, J.J., and McCleary, K.A., J. High Resolut. Chromatogr., 1992, vol. 15, no. 11, p. 705.

    Article  CAS  Google Scholar 

  44. Shearer, R.L., Poole, E.B., and Nowalk, J.B., J. Chromatogr. Sci., 1993, vol. 31, no. 3, p. 82.

    Article  CAS  Google Scholar 

  45. Di Sanzo, F., Bray, W., and Chawla, B., J. High Resolut. Chromatogr., 1994, vol. 17, no. 4, p. 255.

    Article  Google Scholar 

  46. Sung, N.J., Johnson, S.J., and Parrott, S.L., J. High Resolut. Chromatogr., 1994, vol. 17, no. 6, p. 457.

    Article  CAS  Google Scholar 

  47. Ma, X., Sakanishi, K., and Mochida, I., Ind. Eng. Chem. Res., 1994, vol. 33, no. 2, p. 218.

    Article  CAS  Google Scholar 

  48. Andari, M.K., Behbehani, H., and Qabazard, H., Fuel Sci. Technol. Int., 1996, vol. 14, no. 7, p. 897.

    Article  CAS  Google Scholar 

  49. Andari, M.K., Behbehani, H., and Stanislaus, A., Fuel Sci. Technol. Int., 1996, vol. 14, no. 7, p. 939.

    Article  CAS  Google Scholar 

  50. Shearer, R.L. and Meyer, L.M., J. High Resolut. Chromatogr., 1999, vol. 22, no. 7, p. 386.

    Article  CAS  Google Scholar 

  51. Schulz, H., Bohringer, W., Ousmanov, F., and Waller, P., Fuel Process. Technol., 1999, vol. 61, nos. 1–2, p. 5.

    Article  CAS  Google Scholar 

  52. Behbehani, H. and Andari, M.K., Petr. Sci. Technol., 2000, vol. 18, nos. 1–2, p. 51.

    Article  CAS  Google Scholar 

  53. Bacaud, R., Cebollar, V., Membrado, L., Matt, M., Pessayre, S., and Galvez, E., Ind. Eng. Chem. Res., 2002, vol. 41, no. 24, p. 6005.

    Article  CAS  Google Scholar 

  54. Wang, F.C.-Y., Robbins, W.K., Di Sanzo, F.P., and McElroy, F.C., J. Chromatogr. Sci., 2003, vol. 41, no. 10, p. 519.

    Article  CAS  Google Scholar 

  55. Hua, R., Wang, J., Kong, H., Lu, X., and Xu, G., J. High Resolut. Chromatogr., 2004, vol. 27, no. 9, p. 691.

    CAS  Google Scholar 

  56. Nylen, U., Delgado, J.F., Jaras, S., and Boutonnet, M., Fuel Process. Technol., 2004, vol. 86, no. 2, p. 223.

    Article  CAS  Google Scholar 

  57. Behbehania, H., Al-Qallafa, M.A., and El-Dusouquia, O.M.E., Pet. Sci. Technol., 2005, vol. 23, nos. 3–4, p. 219.

    Article  Google Scholar 

  58. Liang, F., Lu, M., Birch, M.E., Keener, T.C., and Liu, Z., J. Chromatogr. A, 2006, vol. 1114, no. 1, p. 145.

    Article  CAS  Google Scholar 

  59. Link, D.D. and Zandhuis, P., Fuel, 2006, vol. 85, no. 4, p. 451.

    Article  CAS  Google Scholar 

  60. Arystanbekova, S.A., Volynskii, A.B., and Prudnikov, I.A., Sovremennye metody gazokhromatograficheskogo analiza nestabil’nogo gazovogo kondensata (Modern Methods of Gas Chromatography Analysis of Unstable Gas Condensate), Moscow Gazprom, 2011.

    Google Scholar 

  61. Arystanbekova, S.A., Lapina, M.S., Volynskii, A.B., Ustyugov, V.S., and Almametov, A.I., J. Anal. Chem., 2012, vol. 67, no. 7, p. 669.

    Article  CAS  Google Scholar 

  62. Mitrevski, B., Amer, M.W., Chaffee, A.L., and Marriott, P.J., Anal. Chim. Acta, 2013, vol. 803, no. 1, p. 174.

    Article  CAS  Google Scholar 

  63. Avila, B.M.F., Pereira, V.B., Gomes, A.O., and Azevedo, D.A., Fuel, 2014, vol. 126, no. 1, p. 188.

    Article  CAS  Google Scholar 

  64. Dijkmans, Th., van Geem, K.M., Djokic, M.R., and Marin, G.B., Ind. Eng. Chem. Res., 2014, vol. 53, no. 40, p. 15436.

    Article  CAS  Google Scholar 

  65. ASTM D 5623-94: Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection, ASTM International, 1994.

  66. Babintseva, M.V., Extended Abstracts of Cand. Sci. (Chem.) Dissertation, Samara Samara State Tech. Univ., 2008.

    Google Scholar 

  67. Arystanbekova, S.A., Volynskii, A.B., Skryabina, A.E., and Gracheva, N.I., in Pererabotka prirodnogo gaza i gazovogo kondensata. Novye razrabotki (Processing of Natural Gas and Gas Condensate: Recent Developments), Kozlov, S.I., Lapidus, A.L., Mamaev, F.V., and Kessel, I.B., Eds., Noscow: VNIIGAZ, 2008, p. 165.

  68. GOST (State Standard) R 56718-2015: Distillates and Stable Gas Condensate. Determination of Sulfur Compounds by Gas Chromatography, Moscow: Standartinform, 2015.

  69. Lyubimenko, V.A. and Kolesnikov, I.M., Khim.Tekhnol. Topliv Masel, 2013, no. 2, p. 29.

    Google Scholar 

  70. Mirzoeva, L.M., Khim.Tekhnol. Topliv Masel, 2014, no. 3, p. 31.

    Google Scholar 

  71. GOST (State Standard) 17323-71: Engine Fuel. Determination of Mercaptan and Hydrogen Sulfide Sulphur Content by Potentiometric Titration, Moscow: Gos. Komitet SSSR po Standartam, 1971.

  72. ASTM D 4294-03: Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy-Dispersive X-ray Fluorescence Spectrometry, ASTM International, 2003.

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Correspondence to A. B. Volynskii.

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Original Russian Text © S.A. Arystanbekova, M.S. Lapina, A.B. Volynskii, 2017, published in Zhurnal Analiticheskoi Khimii, 2017, Vol. 72, No. 5, pp. 399–416.

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Arystanbekova, S.A., Lapina, M.S. & Volynskii, A.B. Determination of individual sulfur-containing compounds in liquid hydrocarbon raw materials and their processing products by gas chromatography. J Anal Chem 72, 473–489 (2017). https://doi.org/10.1134/S1061934817050021

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