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Specific features of the determination of arsenic in soils by electrothermal atomic absorption spectrometry with the injection of suspensions

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Abstract

Problems of the determination of arsenic in soils by electrothermal atomic absorption with the injection of suspensions are discussed. To eliminate an exceptionally high rate of nonselective absorption due to intense evaporation of the inorganic matrix of the sample, the author proposed the reduction of the temperature to arsenic atomization. The optimized temperatures of pyrolysis and atomization steps are 500 and 1800°C, respectively; therein no matrix modifiers were used. The proposed approach was tested on reference samples of soils.

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References

  1. Török, P. and Žemberyová, M., Spectrochim. Acta, 2010, no. 65, p. 291.

    Google Scholar 

  2. Barbosa, F., Jr., Lima, E.C., and Krug, F.J., Analyst, 2000, no. 125, p. 2079.

    Google Scholar 

  3. Lopez-Garcia, I., Sanchez-Merlos, M., and Hernadez-Cordoba, M., Anal. Chim. Acta, 1996, vol. 328, p. 19.

    Article  CAS  Google Scholar 

  4. Burylin, M.Yu., Temerdashev, Z.A., Kaunova, A.A., and Krylova, A.G., Zashchita Okruzhayushchei Sredy v Neftegazovom Komplekse, 2008, no. 2, p. 46.

    Google Scholar 

  5. Souza, A.L. and Oliveira, O.V., J. Anal. Atom. Spectrom., 2010, vol. 25, p. 675.

    Article  CAS  Google Scholar 

  6. Pupyshev, A.A., Analitika i kontrol’, 2008, vol. 12, nos. 3–4, p. 64.

    Google Scholar 

  7. Volynskii, A.B., J. Anal. Chem., 2004, vol. 59, no. 6, p. 502.

    Article  CAS  Google Scholar 

  8. Lima, E.C., Barbosa, F.Jr., Krug, F.J., and Guaita, U., J. Anal. Atom. Spectrom., 1999, vol. 14, p. 1601.

    Article  CAS  Google Scholar 

  9. Tsalev, D.L., J. Anal. Atom. Spectrom., 1995, vol. 10, no. 11, p. 1003.

    Article  CAS  Google Scholar 

  10. Burylin, M.Yu., Temerdashev, Z.A., and Veligodskii, I.M., Zavod. Lab. Diagn. Mater., 2009, vol. 75, no. 11, p. 18.

    Google Scholar 

  11. Pupyshev, A.A., Atomno-absorbtsionnyi spektral’nyi analiz (Atomic Absorption Spectrochemical Analysis), Moscow: Tekhnosfera, 2009.

    Google Scholar 

  12. Nomenclature for the Presentation of Results of Chemical Analysis. IUPAC Recommendations, Pure Appl. Chem., 1994, vol. 66, p. 595.

Download references

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Authors and Affiliations

  1. Faculty of Chemistry and Advanced Technologies, Kuban State University, ul. Stavropol’skaya 149, Krasnodar, 350040, Russia

    M. Yu. Burylin

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  1. M. Yu. Burylin
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Correspondence to M. Yu. Burylin.

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Original Russian Text © M.Yu. Burylin, 2015, published in Zhurnal Analiticheskoi Khimii, 2015, Vol. 70, No. 1, pp. 37–41.

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Burylin, M.Y. Specific features of the determination of arsenic in soils by electrothermal atomic absorption spectrometry with the injection of suspensions. J Anal Chem 70, 39–43 (2015). https://doi.org/10.1134/S1061934815010050

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  • DOI: https://doi.org/10.1134/S1061934815010050

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