Abstract
Highly fluorinated thermally stable polyimide is synthesized and used to modify alumina. The effects of polyimide concentration (10 and 15 wt %) and thermal treatment conditions on the adsorption and chromatographic properties of the prepared adsorbents are studied by the low-temperature adsorption of nitrogen and gas chromatography on packed columns. The adsorbents prepared possess mesoporous structures and ensure the selective separation of permanent gases and hydrocarbons on their simultaneous presence.
Similar content being viewed by others
References
Drugov, Yu.S. and Konopel’ko, L.A., Gazokhromatograficheskii analiz gazov (Gas Chromatography Analysis of Gases), Moscow: Moimpeks, 1995.
Sakodynskii, K.I. and Panina, L.I., Polimernye sorbenty dlya molekulyarnoi khromatografii (Polymer Adsorbents for Molecular Chromatography), Moscow: Nauka, 1977.
Berezkin, V.G., Popova, T.P., Shiryaeva, V.E., Kozlov, S.P., and Vlasenko, E.V., Zavod. Lab. Diagn. Mater., 2003, vol. 69, no. 10, p. 3.
Berezkin, V.G, Popova, T.P., Shiryaeva, V.E., Korolev, A.A., and Malyukova, I.V., Izv. Rus. Akad. Nauk, Ser. Khim., 2002, no. 5, p. 765.
Berezkin, V.G., Mukhina, V.P., Korolev, A.A., Fatkullina, A.F., and Seroshtan, V.A., Zavod. Lab. Diagn. Mater., 2004, vol. 70, no. 5, p. 9.
Yakovleva, E.Yu. and Belotserkovskaya, V.Yu., J. Anal. Chem., 2010, vol. 65, no. 10, p. 1014.
Yakovleva, E.Yu. and Belotserkovskaya, V.Yu., Zh. Fiz. Khim., 2010, vol. 65, no. 10, p. 1039.
Belotserkovskaya, V.Yu. and Yakovleva, E.Yu., Zh. Fiz. Khim., 2011, vol. 9, no. 5, p. 939.
Yakovleva, E.Yu. and Belotserkovskaya, V.Yu., J. Anal. Chem., 2011, vol. 66, no. 6, p. 647.
Vigdergauz, M.S., Gazovaya khromatografiya kak metod issledovaniya nefti (Gas Chromatography as a Method for the Investigation of Petroleum), Moscow: Nauka, 1973.
GOST (State Standard) 13379-82: Determination of Hydrocarbons C1-C6 by Gas Chromatography, 1982.
Modern Practice of Gas Chromatography, Grob, R.L. and Barry, E.F., Eds., Hoboken: Wiley, 2004.
Yakovleva, E.Yu. and Belotserkovskaya, V.Yu., J. Anal. Chem., 2012, vol. 67, no. 9, p. 842.
Alekseeva, O.K. and Amirkhanov, D.M., Ross. Khim. Zh., 2004.
Kazuhiro, T., Hidetoshi, K., Masaaki, O., and Kenichi, O., Polymer, 1992, vol. 33, no. 3, p. 585.
Kim, J.-H., Chang, B.-J., Lee, S.-B., and Kim, S.-Y., J. Membr. Sci., 2002, vol. 69, no. 2, p. 185.
Shundrina, I.K., Vaganova, T.A., Kusov, S.Z., Rodionov, V.I., Karpova, E.V., and Malykhin, E.V., Abstracts of Papers, Materialy Vseross. konf. po makromolek. khimii (Proc. All-Russia Conf. Macromol. Chem.), Ulan-Ude, 2008.
Shundrina, I.K., Vaganova, T.A., Kusov, S.Z., Rodionov, V.I., Karpova, E.V., and Malykhin, E.V., Abstracts of Papers, Materialy Vseross. konf. po makromolek. khimii (Proc. All-Russia Conf. Macromol. Chem.), Ulan-Ude, 2008.
Shundrina, I.K., Vaganova, T.A., Kusov, S.Z., Rodionov, V.I., and Malykhin, E.V., Abstracts of Papers, Materialy Vseross. konf. po makromolek. khimii (Proc. All-Russia Conf. Macromol. Chem.), Ulan-Ude, 2008.
Shundrina, I.K., Vaganova, T.A., Kusov, S.Z., Rodionov, V.I., Karpova, E.V., Koval, V.V., Gerasimova, Yu.V., and Malykhin, E.V., J. Fluorine Chem., 2009, vol. 130, p. 733.
Shundrina, I.K., Vaganova, T.A., Kusov, S.Z., Rodionov, V.I., Karpova, E.V., and Malykhin, E.V., J. Fluorine Chem., 2011, vol. 132, p. 207.
Vaganova, T.A., Shundrina, I.K., Kusov, S.Z., Karpova, E.V., Bagryanskaya, I.Yu., and Malykhin, E.V., J. Fluorine Chem., 2012, vol. 135, p. 129.
Malykhin, E.V., Vaganova, T.A., Karpova, E.V., Kusov, S.Z., Shundrina, I.K., and Rodionov, V.I., Khim. Interesah Ustoich. Razvit., 2011, vol. 19, p. 661.
Handbuch der Gas-Chromatographie, Leibnitz, E. and Struppe, H.G., Eds., Leipzig: Geest and Portig, 1984.
Petsev, N. and Kotsev, N., Spravochnik po gazovoi khromatografii (Handbook of Gas Chromatography), Moscow: Mir, 1987.
Author information
Authors and Affiliations
Additional information
Original Russian Text © E.Yu. Yakovleva, I.K. Shundrina, T.A. Vaganova, 2013, published in Zhurnal Analiticheskoi Khimii, 2013, Vol. 68, No. 12, pp. 1171–1178.
Rights and permissions
About this article
Cite this article
Yakovleva, E.Y., Shundrina, I.K. & Vaganova, T.A. Specific features of the separation of inorganic and organic compounds on alumina modified with fluorinated polyimide. J Anal Chem 68, 1044–1051 (2013). https://doi.org/10.1134/S1061934813100110
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1061934813100110