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Journal of Analytical Chemistry

, Volume 68, Issue 11, pp 959–960 | Cite as

Determination of phthalate esters content in plastic articles: Comparison of extraction methods

  • Monika Gawlik-Jędrysiak
Articles

Abstract

Two variants of solvent extraction method (by Soxhlet and ultrasonic) for phthalate esters (DEHP) recoveries in PVC samples were compared. Solvent and extraction time for both techniques were also studied. DEHP content was quantified by GC-MS. The results obtained were compared using statistical methods (LSD test, t-test). 16-Hours DCM Soxhlet and 2-h DCM ultrasonic extraction methods were more convenient with respect to recovery, precision and practicability.

Keywords

phthalate ester GC-MS extraction PVC 

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Copyright information

© Pleiades Publishing, Ltd. 2013

Authors and Affiliations

  • Monika Gawlik-Jędrysiak
    • 1
  1. 1.Laboratory of Material Engineering and EnvironmentInstitute of Mining Technology KOMAGGliwicePoland

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