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Determination of the phenol index of water by stepwise injection analysis with offline preconcentration by extraction chromatography

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Abstract

A procedure for the photometry determination of the phenol index of aqueous media is developed, which involves the preliminary separation of alkylphenols and their derivatives from water samples in sampling. Samples are filtered through an extraction chromatography column containing tributyl phosphate as an active component of the stationary phase followed by their quantification under the conditions of stepwise injection analysis. The detection limit of the method is 0.1 μg/L for simple phenol.

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Authors and Affiliations

  1. St. Petersburg State University, Universitetskii pr. 26, St. Petersburg, 198504, Russia

    A. V. Bulatov, E. A. Mikhailova, I. I. Timofeeva, A. L. Moskvin & L. N. Moskvin

Authors
  1. A. V. Bulatov
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  2. E. A. Mikhailova
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  3. I. I. Timofeeva
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  4. A. L. Moskvin
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  5. L. N. Moskvin
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Additional information

Original Russian Text © A.V. Bulatov, E.A. Mikhailova, I.I. Timofeeva, A.L. Moskvin, L.N. Moskvin, 2013, published in Zhurnal Analiticheskoi Khimii, 2013, Vol. 68, No. 1, pp. 18–21.

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Bulatov, A.V., Mikhailova, E.A., Timofeeva, I.I. et al. Determination of the phenol index of water by stepwise injection analysis with offline preconcentration by extraction chromatography. J Anal Chem 68, 15–18 (2013). https://doi.org/10.1134/S1061934812110032

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  • DOI: https://doi.org/10.1134/S1061934812110032

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