Journal of Analytical Chemistry

, Volume 66, Issue 12, pp 1196–1200 | Cite as

Determination of the chemical composition of Spice aromatic smoking blends by chromatography-mass spectrometry

  • S. V. Nekhoroshev
  • V. P. Nekhoroshev
  • M. N. Remizova
  • A. V. Nekhorosheva
Articles

Abstract

The composition of methanol extracts of Spice aromatic smoking blends was studied by chromatography-mass spectrometry. The following compounds from the group of new synthetic cannabinoids were identified: 1-pentyl-3-(1-naphthoyl)indol, 1-butyl-3-(1-naphthoyl)indol, 1-hexyl-3-(1-naphthoyl)indol, and 3-[4-(1,1-dimethyloctyl)-2-hydroxyphenyl]cyclohexan-1-ol and its optical isomer. The smoking blends also contained caffeine, glycerol, vitamin E, vanillin, ethylvanillin, and menthol.

Keywords

smoking blends synthetic cannabinoids chromatography-mass spectrometry identification retention indices 

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References

  1. 1.
    Kuritel’nye smesi Spais gold, Spais daimond. Enteogeny (Smoking Blends Spice Golg, Spice Diamond. Entheogens), Elektronnyi resurs (Electronic Resource), http://www.moscowspice.ru/; The Smog—spice, spaisy i miksy. Spice Golg, Spice Diamond, Spice Silver (The Smog: Spice, Spices, and Mixes. Spice Golg, Spice Diamond, Spice Silver), Elektronnyi resurs (Electronic Resource), http://www.thesmog.ru/.
  2. 2.
    Ob usilenii nadzora za realizatsiei kuritel’nykh smesei: Postanovlenie 23 ot 09.04.2009 g. glavnogo gosudarstvennogo sanitarnogo vracha RF Federal’noi sluzhby po nadzoru v sfere zashchity prav potrebitelei i blagopoluchiya cheloveka (On Strengthening the Supervision of Smoking Mixtures: Ordinance no. 23 of Chief State Sanitary Doctor of the Russian Federal Service for Supervision of Consumer Rights Protection and Human Welfare, April 9, 2009), Moscow, 2009; Rossiiskaya gazeta, no. 4892, April 17, 2009.Google Scholar
  3. 3.
    Lindigkeit, R., Boehme, A., Eiserloh, I., Luebbecke, M., Wiggermann, M., Ernst, L., and Beuerle, T., Forensic Sci. Int., 2009, no. 191, p. 58.Google Scholar
  4. 4.
    Auwärter, V., Dresen, S., Weinmann, W., Muller, M., Pütz, M., and Ferreirós, N., J. Mass Spectrom., 2009, no. 44, p. 832.Google Scholar
  5. 5.
    Bezuglov, V.V., Bobrov, M.Yu., and Archakov, A.V., Bioaktivnye amidy zhirnykh kislot (Biologically Active Fatty Acid Amides), Elektronnyi resurs (Electronic Resource), http://www.scritube.com/limba/rusa/552421816.php
  6. 6.
    O vnesenii izmenenii v nekotorye postanovleniya Pravitel’stva Rossiiskoi Federatsii po voprosam, svyazannym s oborotom narkoticheskikh sredstv: Postanovlenie Pravitel’stva RF (On Amendments to Some Decisions of the Government of the Russian Federation on Issues Related to the Traffic of Narcotic Drugs: Ordinance of The Government of the Russian Federation), Moscow:, 2009; Rossiiskaya gazeta, no. 5083, January 14, 2010.Google Scholar
  7. 7.
    Vigdergauz, M.S., Raschety v gazovoi khromatografii (Calculations in Gas Chromatography), Moscow: Khimiya, 1978.Google Scholar

Copyright information

© Pleiades Publishing, Ltd. 2011

Authors and Affiliations

  • S. V. Nekhoroshev
    • 1
  • V. P. Nekhoroshev
    • 2
  • M. N. Remizova
    • 3
  • A. V. Nekhorosheva
    • 3
  1. 1.Russian Federal Service for Drug Control in Khanty-Mansi Autonomous District-YugraKhanty-MansiiskRussia
  2. 2.Faculty of Chemistry and TechnologySurgut State UniversitySurgut, Khanty-Mansi Autonomous DistrictRussia
  3. 3.Faculty of Natural Sciences and GeographyNizhnevartovsk State Humanitarian UniversityNizhnevartovsk, Khanty-Mansi Autonomous DistrictRussia

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