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Determination of impurities in high-purity hydrogen sulfide by gas chromatography-mass spectrometry using gas adsorption capillary columns

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Abstract

Gas chromatography-mass spectrometry has been used to study the impurity composition of high-purity hydrogen sulfide. Impurities of atmospheric gases, COS,CS2, SO2, benzene, toluene, thiophene, and its homologues have been detected. Detection limits of impurities are 10−7-10−5 vol %.

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Authors and Affiliations

  1. Institute of High-Purity Substance, Russian Academy of Sciences, ul. Tropinina 49, Nizhnii Novgorod, 603950, Russia

    V. A. Krylov, A. Yu. Sozin & O. Yu. Chernova

  2. Department of Chemistry, Nizhni Novgorod State University, pr. Gagarina 23, Nizhnii Novgorod, 603950, Russia

    V. A. Krylov

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  1. V. A. Krylov
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  2. A. Yu. Sozin
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  3. O. Yu. Chernova
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Original Russian Text © V.A. Krylov, A.Yu. Sozin, O.Yu. Chernova, 2011, published in Zhurnal Analiticheskoi Khimii, 2011, Vol. 66, No. 6, pp. 652–657.

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Krylov, V.A., Sozin, A.Y. & Chernova, O.Y. Determination of impurities in high-purity hydrogen sulfide by gas chromatography-mass spectrometry using gas adsorption capillary columns. J Anal Chem 66, 634–640 (2011). https://doi.org/10.1134/S1061934811060104

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  • DOI: https://doi.org/10.1134/S1061934811060104

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