Abstract
The impurities in high-purity carbon tetrachloride (CCl 4 ) were determined by gas chromatography-mass spectrometry (GC-MS). The use of chromatography of near-saturated vapors allowed the injection of samples up to 1 μL into a capillary column and to achieve specific column efficiency in an isothermal mode of 221,000 t.p./m. The detection limits for impurities were 1 × 10−1 to 1 × 10−8 wt %.
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Original Russian Text © V.A. Krylov, P.V. Mosyagin, A.V. Krylov, A.Yu. Sozin, L.B. Nushtaeva, 2010, published in Zhurnal Analiticheskoi Khimii, 2010, Vol. 65, No. 10, pp. 1084–1090.
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Krylov, V.A., Mosyagin, P.V., Krylov, A.V. et al. Determination of impurities in high-purity carbon tetrachloride by gas chromatography-mass spectrometry. J Anal Chem 65, 1061–1067 (2010). https://doi.org/10.1134/S1061934810100126
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DOI: https://doi.org/10.1134/S1061934810100126