Abstract
The main peculiarities and difficulties in the implementation of circulation chromatography are considered. The most impressive results obtained with the use of circulation liquid chromatography for the separation of isotopically substituted and isomeric organic compounds are given. The possibility of the preparative separation of the optical isomers of amino acid derivatives was demonstrated for the first time; thus, a new technique for the separation of optical isomers was developed. The capabilities of the circulation versions of gas-liquid and gas-adsorption chromatography are considered in detail. The possibility of the ultrafine separation of isotopically substituted compounds that differ by only one isotope atom, such as benzene and monodeuterobenzene, was demonstrated.
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References
Martin, A.J.P., in Vapour phase chromatography, Desty, D.H., Ed., London: Butterworths, 1957.
Martin, A.J.P., Gas Chromatography, Coates, V.S., et al., Eds., New York: Academic, 1958.
Porter, R.S. and Johnson, J.F., Nature, 1959, vol. 183, p. 391.
Porter, R.S. and Johnson, J.F., Nature, 1959, vol. 184, p. 978.
Porath, J. and Bennich, H., Arch. Biochem. Biophys., 1962, no. 1(suppl.), p. 152.
Yoshida, T., Chi-Kuen, Shu., and Theimer, E.T., J. Chromatogr., 1977, vol. 137, no. 2, p. 461.
Bombaugh, K.J., Dark, W.A., and Levangie, R.F., J. Chromatogr. Sci., 1969, vol. 7, no. 1, p. 42.
Spedding, E., Powell, J.W., and Svec, H., J. Am. Chem. Soc., 1955, vol. 77, no. 23, p. 6125.
Andreev, B.M., Boreskov, G.K., and Katal’nikov, S.G., Khimich. promyshl., 1961, no. 6, p. 389.
Lesec, J., Lafuma, F., and Quivoron, C., J. Chromatogr. Sci., 1974, vol. 12, p. 683.
Lesec, J., Lafuma, F., and Quivoron, C., J. Chromatogr., 1977, vol. 138, no. 1, p. 89.
Wartim, R., Verillon, F., Eon, C., and Guiochon, G., J. Chromatogr., 1976, vol. 125, no. 1, p. 17.
Pokorny, R., Lukas, R., Yanca, J., and Kolinsky, M., J. Chromatogr., 1978, vol. 148, no. 1, p. 183.
Kucera, P. and Manius, G., J. Chromatogr., 1981, vol. 219, no. 1, p. 1.
Bombaugh, R.J. and Levangie, R.F., J. Chromatogr. Sci., 1970, vol. 8, p. 560.
Bombaugh, R.J. and Levangie, R.F., Sep. Sci., 1970, no. 5(6), p. 751.
Henry, R.A., Byrne, S.H., and Hudson, D.R., J. Chromatogr. Sci., 1974, vol. 12, p. 197.
Little, J.N., Cotter, R.L., Prendergast, J.A., and Patrick, D., J. Chromatogr., 1976, vol. 126, p. 439.
Minaric, M., Popl, M., and Mostecky, J., J. Chromatogr. Sci., 1981, vol. 19, p. 250.
Coq, B.E., Cretier, G., Rocca, J.L., and Vialle, B.J., J. Liq. Chromatogr., 1981, vol. 4, no. 2, p. 237.
Chizhkov, V.P., Zhurn. anal. khim., 1972, vol. 27, p. 1383.
Chizhkov, V.P., Matyukov, A.A., Gurevich, Ya.A., and Litvin, E.F., Zhurn. fiz. khim., 1969, vol. 43, p. 1053.
Snyder, L.R., J. Chromatogr. Sci., 1969, vol. 7, p. 352.
Chizhkov, V.P., Usorov, M.I., and Sinitsina, L.A., Zavod. lab., 1971, vol. 37, p. 1286.
Chizhkov, V.P., Matyukov, A.A., Gurevich, Ya.A., and Litvin, E.F., Zavod. lab., 1969, vol. 35, p. 1446.
Chizhkov, V.P. and Usorov, M.I., Zavod. lab., 1971, vol. 35, p. 1281.
Chizhkov, V.P., Litvin, E.F., Usorov, M.I., Yakushina, L.M., and Matyukov, A.A., Izv. Akad. Nauk SSSR, Ser.: Khim., 1971, no. 5, p. 1154.
Usorov, M.I., Cand. Sci. (Chem.) Dissertation, Moscow: IOKh AN SSSR, 1972.
Zabokritskii, M.P., Rudenko, B.A., and Chizhkov, V.P., Izv. Akad. Nauk SSSR, Ser. Khim., 1977, no. 7, p. 1627.
Skornyakov, E.P., Sakodynskii, K.I., and Chizhkov, V.P., Zhurn. fiz. khim., 1966, vol. 40, p. 600.
Chizhkov, V.P. and Sinitsina, L.A., Zhurn. anal. khim., 1974, vol. 29, p. 600.
Chizhkov, V.P. and Sinitsina, L.A., J. Chromatogr., 1975, vol. 104, no. 2, p. 327.
Chizhkov, V.P., Yushina, G.A., and Litvin, E.F., Zhurn. fiz. khim., 1978, vol. 52, p. 475.
Zabokritskii, M.P., Rudenko, B.A., and Chizhkov, V.P., in Analiticheskoe i preparativnoe primenenie khromatografii (Analytical and Preparative Applications of Chromotography), Moscow: NIITEKhIM, 1980, p. 62.
Chizhkov, V.P. and Sinitsina, L.A., Zhurn. fiz. khim., 1974, vol. 48, p. 142.
Chizhkov, V.P., Rudenko, B.A., Sinitsina, L.A., and Yushina, G.A., Izv. Akad. Nauk SSSR, Ser.: Khim., 1975, no. 6, p. 1207.
Reid, A.M., J. Chromatogr. Sci., 1976, vol. 14, p. 203.
Min, R.S., Aksenov, V.S., Vinogradov, M.G., and Nikishin, G.I., Izv. Akad. Nauk SSSR, Ser.: Khim., 1979, no. 10, p. 2292.
Zabokritskii, M.P., Chizhkov, V.P., and Rudenko, B.A., Usp. Khim., 1984, vol. 53, no. 9, p. 1572.
Zabokritskii, M.P., Pavlov, S.S., Rudenko, B.A., and Chizhkov, V.P., USSR Inventorís Certificate no. 756289, Byull. Izobret., 1980, no. 30.
Zabokritskii, M.P., Bukin, V.A., and Rudenko, B.A., Izv. Akad. Nauk SSSR, Ser.: Khim., 1982, no. 11, p. 2277.
Anteunis, M. and Alderweireldt, F., Bull. Soc. Chim. Belg., 1964, vol. 73, p. 903.
Rammelaere, Y. and Anteunis, M., J. High Resolut. Chromatogr. Chromatogr. Commun., 1970, vol. 79, p. 11.
Willi, W.E., Binsch, G., and Eliel, E.L., J. Am. Chem. Soc., 1970, vol. 92, no. 18, p. 5394.
Kametani, F. and Sumi, Y., Chem. Pharm. Bull., 1972, vol. 20, p. 1479.
Gil-Av, E. and Feibush, B., Tetrahedron Lett., 1967, vol. 35, no. 20, p. 3345.
Feibush, B., Chem. Commun., 1971, no. 11, p. 544.
Frank, H., Nickolson, G.J., and Bayer, E., J. Chromatogr. Sci., 1977, vol. 15, p. 176.
Saed, T., Sandra, P., and Verzele, M., J. Chromatogr., 1979, vol. 186, p. 611.
Oi, N., Hiroaki, J., and Shimada, H., Bunseku Kagaku (Japan Analyst), 1979, vol. 28, p. 125.
Oi, N., Hiroaki, J., Shimada, H., Horiba, M., and Kitahara, H., Bunseku Kagaku (Japan Analyst), 1980, vol. 29, p. 270.
Lochmuller, C.H. and Souter, R.W., J. Chromatogr., 1973, vol. 87, p. 243.
Bonner, W.A., Van Dort, M.A., and Flores, J., Anal. Chem., 1974, vol. 46, no. 14, p. 2104.
Charles, R., Beitler, U., Feibush, B., and Gil-Av, E., J. Chromatogr., 1975, vol. 112, p. 121.
Oi, N., Horiba, M., and Kitahara, H., J. Chromatogr., 1980, vol. 202, no. 2, p. 299.
Zabokritskii, M.P., Rudenko, B.A., Chizhkov, V.P., Mitsner, B.I., and Zvonkova, E.N., Izv. Akad. Nauk SSSR, Ser.: Khim., 1981, no. 5, p. 1045.
Zabokritskii, M.P., Rudenko, B.A., and Chizhkov, V.P., Dokl. Akad. Nauk SSSR, 1982, vol. 263, p. 1155.
Chizhkov, V.P. and Yushina, G.A., Zhurn. fiz. khim., 1977, vol. 51, p. 737.
Chizhkov, V.P., Yushina, G.A., and Ferapontov, V.A., Zavod. lab., 1977, vol. 43, p. 943.
Jennings, W., Settlage, J.A., and Miller, R.J., J. High Resolut. Chromatogr. Chromatogr. Commun., 1979, vol. 2, p. 441.
Jennings, W., Settlage, J.A., Miller, R.J., and Raabe, O.G., J. Chromatogr., 1979, vol. 186, p. 189.
Sterkhov, N.V. and Chizhkov, V.P., Izv. Akad. Nauk SSSR, Ser.: Khim., 1986, no. 9, p. 2019.
Chizhkov, V.P., Pavlov, S.S., Sterkhov, N.V., Ravicovich, V.M., Litvin, E.F., and Varivonchik, E.A., Talanta, 1987, vol. 34, no. 1, p. 227.
Chizhkov, V.P. and Sterkhov, N.V., Kontseptsiya i teoriya kolonochnoi zhidkostnoi khromatografii s mnogokratnym kontsentrirovaniem razdelyaemykh komponentov (Conception and Theory of Column Liquid Chromatography with Multiple Preconcentration of Separated Components), Moscow: IOKh AN SSSR, 1995.
Chizhkov, V.P. and Sterkhov, N.V., Zhurn. fiz. khim., 1997, vol. 71, no. 9, p. 1678.
Leutert, T.H., La Vecchia, L., Ossola, F., Richert, F., Schmidt, A., (Electronnyi resurs), www.nibr.novartis.com/OurScienceDiscoveryResearch/CentralTechnologies/Publ (Electronic Resource).
Tsirkulyatsionnaya khromatografiya (Circulation Chromatography), (Electronnyi resurs), www.uns.ssu.samara.ru/bnook1/1_4.html (Electronic Resource).
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Original Russian Text © B.A. Rudenko, 2009, published in Zhurnal Analiticheskoi Khimii, 2009, Vol. 64, No. 6, pp. 565–570.
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Rudenko, B.A. Circulation chromatography. J Anal Chem 64, 547–552 (2009). https://doi.org/10.1134/S1061934809060021
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DOI: https://doi.org/10.1134/S1061934809060021