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Electroinjection determination of aluminum in aqueous solutions

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Abstract

A procedure is proposed for determining aluminum(III) in water over a concentration range of 0.1–2.0 mg/L in the presence of commensurable amounts of iron(III) using electroinjection analysis. The following parameters were varied in the experiments: the composition and pH of a working buffer solution, the reagent-to-metal concentration ratio, the time of sample injection, the composition of a buffer solution in sample preparation for analysis, the concentration of the reagent (Xylenol Orange), and the reaction time. As a result of this, the sensitivity and selectivity of determining aluminum were improved as compared with the currently available procedures.

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Authors and Affiliations

  1. St. Petersburg State University (Petrodovrets Branch), Universitetskii pr. 26, Petrodvorets, 198504, Russia

    O. I. Markova & T. G. Nikitina

  2. OAO TsKP Analiticheskaya Spektrometriya, ul, Gzhatskaya 27-A, St. Petersburg, 195220, Russia

    L. N. Moskvin & V. P. Andreev

Authors
  1. O. I. Markova
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  2. T. G. Nikitina
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  3. L. N. Moskvin
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  4. V. P. Andreev
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Original Russian Text © O.I. Markova, T.G. Nikitina, L.N. Moskvin, V.P. Andreev, 2006, published in Zhurnal Analiticheskoi Khimii, 2006, Vol. 61, No. 2, pp. 192–198.

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Markova, O.I., Nikitina, T.G., Moskvin, L.N. et al. Electroinjection determination of aluminum in aqueous solutions. J Anal Chem 61, 179–185 (2006). https://doi.org/10.1134/S1061934806020158

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  • DOI: https://doi.org/10.1134/S1061934806020158

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