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Optimization of hydrothermally synthesized LiFePO4 nanoscaled particles for lithium-ion batteries

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Abstract

Phase-pure nano-LiFePO4 was successfully fabricated under hydrothermal condition at different temperatures. We found that the obtained particle morphologies and sizes were temperature-dependent. Compared with other samples, the as-received LiFePO4 synthesized at 200°C for 3 h presented monodisperse state. Moreover, this product possessed excellent electrochemical performance and cycling stability after annealing at 700°C for 1 h with glucose as carbon source.

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References

  1. Bai, Y.M., Chen, H., and Han, Sh.-Ch., Russ. J. Electrochem., 2011, vol. 47, no. 1, p. 84.

    Article  CAS  Google Scholar 

  2. Yuan, S.Q. and Dai K.J., Russ. J. Electrochem., 2010, vol. 47, no. 9, p. 1068.

    Google Scholar 

  3. Huang, W.Q., Qing, C., and Qin, X., Russ. J. Electrochem., 2010, vol. 46, no. 3, p. 359.

    Article  CAS  Google Scholar 

  4. Yuan, S.Q. and Dai, K.J., Russ. J. Electrochem., 2010, vol. 47, no. 12, p. 1389.

    Article  Google Scholar 

  5. Huang, W.Q., Qing, C., and Qin, X., Russ. J. Electrochem., 2010, vol. 46, no. 2, p. 175.

    Article  CAS  Google Scholar 

  6. Padhi, A.K., Nanjundaswamy, K.S., and Goodenough, J.B., J. Electrochem. Soc., 1997, vol. 144, p. 1188.

    Article  CAS  Google Scholar 

  7. Gibot, P., Cabanas, M.C., Laffont, L., Levasseur, S., Carlach, P., Hamelet, S.P., Tarascon, J.M., and Masquslier, C., Nat. Mater., 2008, vol. 7, p. 741.

    Article  CAS  Google Scholar 

  8. Zhao, J.Q., He, J.P., Zhou, J.H., Guo, Y.X., Wang, T., Wu, S.C., Ding, X.C., Huang, R.M., and Xue, H.R., J. Phys. Chem. C, 2011, vol. 115, p. 2888.

    Article  CAS  Google Scholar 

  9. Kang, B. and Ceder, G., Nature, 2009, vol. 458, p. 190.

    Article  CAS  Google Scholar 

  10. Belharouak, I., Johnson, C., and Amine, K., Electrochem. Commun., 2005, vol. 7, p. 983.

    Article  CAS  Google Scholar 

  11. Wang, G.X., Bewlay, S., Yao, J., Ahn, J.H., Dou, S.X., and Liu, H.K., Electrochem. Solid-State Lett., 2004, vol. 7, p. 503.

    Article  Google Scholar 

  12. LaMer, V.K. and Dinegar, R.H., J. Am. Chem. Soc., 1950, vol. 72, p. 4847.

    Article  CAS  Google Scholar 

  13. Qin, X., Wang, X.H., Xiang, H.M., Xie, J., Li, J.J., and Zhou, Y.C., J. Phys. Chem. C, 2010, vol. 114, p. 16806.

    Article  CAS  Google Scholar 

  14. Yang, S.F. and Zavalij, P.Y., Whittingham, M.S., Electrochem. Commun., 2001, vol. 3, p. 505.

    Article  CAS  Google Scholar 

  15. Qin, X., Wang, X.H., Xie, J., and Wen, L., J. Mater. Chem., 2011, vol. 21, p. 12444.

    Article  CAS  Google Scholar 

  16. Chen J.J. and Whittingham, M.S., Electrochem. Commun., 2006, vol. 8, p. 855.

    Article  CAS  Google Scholar 

  17. Qin, X., Wang, J.M., Xie, J., Li, F.Z., Wen, L., and Wang, X.H., Phys. Chem. Chem. Phys., 2012, vol. 14, p. 2669.

    Article  CAS  Google Scholar 

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Correspondence to Jingqing Gao.

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Published in Russian in Elektrokhimiya, 2013, Vol. 49, No. 5, pp. 525–529.

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Qiao, Y., Guo, H., Liu, G. et al. Optimization of hydrothermally synthesized LiFePO4 nanoscaled particles for lithium-ion batteries. Russ J Electrochem 49, 466–469 (2013). https://doi.org/10.1134/S1023193513050091

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  • DOI: https://doi.org/10.1134/S1023193513050091

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