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Mesoporous MgO: Synthesis, physico-chemical, and catalytic properties

  • Physical Chemistry of Nanoclusters and Nanomaterials
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Abstract

Mesoporous MgO was obtained via the hydrothermal synthesis using both ionogenic and non-ionogenic surfactants as structure-directing templates. The materials prepared were characterized by SEM, BET-N2, XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide particles well shaped as rectangular parallelepipeds. Magnesium oxide samples have the specific surface area of 290–400 m2/g and pore sizes of 3.3–4.1 nm. Their mesoporous structure remained unchanged after calcination up to 350°C. Catalytic activity of mesoporous MgO was studied in acetone condensation reaction.

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Authors and Affiliations

  1. Department of Chemistry, Moscow State University, Moscow, 119991, Russia

    A. A. Maerle, I. A. Kasyanov, I. F. Moskovskaya & B. V. Romanovsky

Authors
  1. A. A. Maerle
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  2. I. A. Kasyanov
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  3. I. F. Moskovskaya
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  4. B. V. Romanovsky
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Corresponding author

Correspondence to I. F. Moskovskaya.

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The article was translated by the authors.

Published in Russian in Zhurnal Fizicheskoi Khimii, 2016, Vol. 90, No. 6, pp. 902–906.

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Maerle, A.A., Kasyanov, I.A., Moskovskaya, I.F. et al. Mesoporous MgO: Synthesis, physico-chemical, and catalytic properties. Russ. J. Phys. Chem. 90, 1212–1216 (2016). https://doi.org/10.1134/S0036024416060108

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  • DOI: https://doi.org/10.1134/S0036024416060108

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