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Modification and dispersion of multi-walled carbon nanotubes in water

  • Physical Chemistry of Nanoclusters and Nanomaterials
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Abstract

In the present work, the decorated purified raw multi-walled carbon nanotubes (R-MWCNTs) were obtained by chemical modification (CM) by treatment with concentrated sulfuric acid and concentrated nitric acid mixture with a certain volume ratio of 1: 3. The R-MWCNTs and CM-MWCNTs samples were investigated by X-ray Diffraction (XRD) analysis and Fourier transform infrared spectroscopy (FT-IR). The prepared MWCNTs were homogeneously dispersed in water using a commercial surfactant (Polyvinyl pyrrolidone, (PVP)) and ultra-sonication. The dispersion of MWCNTs was obtained by UV-Vis analysis. The results show that chemical modification purified MWCNTs and more effective functional groups were attached on the surface of MWCNTs. Meanwhile, R-MWCNTs and CM-MWCNTs were uniformly distributed in aqueous PVP solution and the dispersion of CM-MWCNTs in water was better.

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References

  1. S. Iijima, Nature 354, 56 (1991).

    Article  CAS  Google Scholar 

  2. S. Iijima, Phys. B: Condens. Matter 323, 1 (2002).

    Article  CAS  Google Scholar 

  3. J. P. Salvetat, J. M. Bonard, M. H. Thomson, et al., Appl. Phys. A 69, 255 (1999).

    Article  CAS  Google Scholar 

  4. M. F. Yu, O. Lourie, M. J. Dyer, et al., Science 287(5453), 637 (2000).

    Article  CAS  Google Scholar 

  5. M. Mazaheri, D. Mari, Z. R. Hesabi, et al., Compos. Sci. Technol. 71, 939 (2011).

    Article  CAS  Google Scholar 

  6. M. R. Ayatollahi, S. Shadlou, and M. M. Shokrieh, Mater. Des. 32, 2115 (2011).

    Article  CAS  Google Scholar 

  7. C. Liu, Y. Y. Fan, M. Liu, et al., Science 286(5442), 1127 (1999).

    Article  CAS  Google Scholar 

  8. S. Rather, R. Zacharia, S. W. Hwang, et al., Chem. Phys. Lett. 441, 261 (2007).

    Article  CAS  Google Scholar 

  9. F. Shunjiro, S. Honda, H. Machida, et al., Appl. Phys. Lett. 90, 153108 (2007).

    Article  Google Scholar 

  10. E. Frackowiak, Phys. Chem. Chem. Phys. 9, 1774 (2007).

    Article  CAS  Google Scholar 

  11. D. N. Futaba, K. Hata, T. Yamada, et al., Nature Mater. 5, 987 (2006).

    Article  CAS  Google Scholar 

  12. H. J. Dai, J. H. Hafner, A. G. Rinzler, et al., Nature 384, 147 (1996).

    Article  CAS  Google Scholar 

  13. S. Ravindran, S. Chaudhary, B. Colburn, et al., Nano Lett. 3, 447 (2003).

    Article  CAS  Google Scholar 

  14. C. Park, Z. Ounaies, K. A. Watson, et al., Chem. Phys. Lett. 364, 303 (2002).

    Article  CAS  Google Scholar 

  15. G. Y. Li, P. M. Wang, and X. Zhao, Carbon 43, 1239 (2005).

    Article  CAS  Google Scholar 

  16. G. Y. Li, P. M. Wang, and X. Zhao, Chem. Concr. Compos. 29, 377 (2007).

    Article  CAS  Google Scholar 

  17. B. Wang, Y. Han, K. Song, et al., J. Nanosci. Nanotech. 12, 4664 (2012).

    Article  CAS  Google Scholar 

  18. B. Wang, Y. Han, and T. Zhang, J. Nanosci. Nanotech. 12, 8415 (2012).

    Article  CAS  Google Scholar 

  19. Y. Gogotsi, N. Naguib, and J. A. Libera, Chem. Phys. Lett. 365, 354 (2002).

    Article  CAS  Google Scholar 

  20. A. Rasheed, J. Y. Howe, M. D. Dadmun, et al., Carbon 45, 1072 (2007).

    Article  CAS  Google Scholar 

  21. J. Zhang, H. Zou, Q. Qing, et al., J. Phys. Chem. B 107, 3712 (2003).

    Article  CAS  Google Scholar 

  22. J. M. Zhou, H. Y. Li, G. D. Lin, et al., Acta Phys. Chem. Sin. 26, 3080 (2010).

    CAS  Google Scholar 

  23. X. Zhou, L. Yu, Q. Guo, et al., New Chem. Mater. 37(6), 61 (2009).

    CAS  Google Scholar 

  24. L. Jiang, L. Gao, and J. Sun, J. Colloid. Interface Sci. 260, 89 (2003).

    Article  CAS  Google Scholar 

  25. I. D. Rosca, F. Watari, M. Uo, et al., Carbon 43, 3124 (2005).

    Article  CAS  Google Scholar 

  26. T. Saito, K. Matsushige, and K. Tanaka, Phys. B: Condens. Matter 323, 2802002 (2002).

    Google Scholar 

  27. K. A. Wepasnick, B. A. Smith, K. E. Schrote, et al., Carbon. 49, 24 (2011).

    Article  CAS  Google Scholar 

  28. L. Vaisman, H. D. Wagner, and G. Marom, Adv. Colloid. Interface Sci. 37(128–130), 37 (2006).

    Article  Google Scholar 

  29. M. S. Strano, V. C. Moore, M. K. Miller, et al., J. Nanosci. Nanotech. 3, 81 (2003).

    Article  CAS  Google Scholar 

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Correspondence to Y. M. Zhang.

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He, Z.H., Gao, G.B. & Zhang, Y.M. Modification and dispersion of multi-walled carbon nanotubes in water. Russ. J. Phys. Chem. 88, 1191–1195 (2014). https://doi.org/10.1134/S0036024414070176

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  • DOI: https://doi.org/10.1134/S0036024414070176

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