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Production of HfB2–SiC (10–65 vol % SiC) Ultra-High-Temperature Ceramics by Hot Pressing of HfB2–(SiO2–C) Composite Powder Synthesized by the Sol–Gel Method

  • Synthesis and Properties of Inorganic Compounds
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Abstract

The formation of HfB2–SiC (10–65 vol % SiC) ultra-high-temperature ceramics by hot pressing of HfB2–(SiO2–C) composite powder synthesized by the sol–gel method was studied. By the example of HfB2–30 vol % SiC ceramic, it was shown that the synthesis of nanocrystalline silicon carbide is completed at temperatures of as low as ≥1700°C (crystallite size 35–39 nm). The production of the composite materials with various contents of fine silicon carbide at 1800°C demonstrated that the samples of the composition HfB2–SiC (20–30 vol % SiC) are characterized by the formation of SiC crystallites of the minimum sizes (36–38 nm), by the highest density (89%), and by higher oxidation resistance during heating in an air flow to 1400°C.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, 119991, Russia

    E. P. Simonenko, N. P. Simonenko, V. G. Sevastyanov & N. T. Kuznetsov

  2. Institute of Chemistry, Far-Eastern Branch, Russian Academy of Sciences, Vladivostok, 690022, Russia

    E. K. Papynov

  3. Far-Eastern Federal University, Vladivostok, 690950, Russia

    E. K. Papynov & E. A. Gridasova

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  1. E. P. Simonenko
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  2. N. P. Simonenko
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  3. E. K. Papynov
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  4. E. A. Gridasova
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  5. V. G. Sevastyanov
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  6. N. T. Kuznetsov
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Correspondence to E. P. Simonenko.

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Original Russian Text © E.P. Simonenko, N.P. Simonenko, E.K. Papynov, E.A. Gridasova, V.G. Sevastyanov, N.T. Kuznetsov, 2018, published in Zhurnal Neorganicheskoi Khimii, 2018, Vol. 63, No. 1, pp. 3–18.

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Simonenko, E.P., Simonenko, N.P., Papynov, E.K. et al. Production of HfB2–SiC (10–65 vol % SiC) Ultra-High-Temperature Ceramics by Hot Pressing of HfB2–(SiO2–C) Composite Powder Synthesized by the Sol–Gel Method. Russ. J. Inorg. Chem. 63, 1–15 (2018). https://doi.org/10.1134/S0036023618010187

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