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Effect of microwave exposure on the morphology of calcium hydroxyapatite nanocrystals synthesized from aqueous solutions

  • Synthesis and Properties of Inorganic Compounds
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Abstract

The results of physicochemical examination (chemical analysis, XRD, IR spectroscopy) of the products synthesized in the Ca(OH)2–H3PO4–H2O system under microwave exposure are used to analyze the composition–synthesis conditions–structure–dispersion–properties relationships and to determine the effect of microwave irradiation on the size and morphology of the synthesized calcium hydroxyapatite (Ca10(PO4)6(OH)2) nanocrystals.

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References

  1. N. A. Zakharov and V. T. Kalinnikov, Fundamental Science for Medicine. Biophysical Medical Technologies, Ed. by A. I. Grigor’ev and Yu. A. Vladimirov (MAKS Press, Moscow, 2015), Vol. 2 [in Russian].

  2. L. L. Hench, J. Am. Ceram. Soc. 74, 1487 (1991).

    Article  CAS  Google Scholar 

  3. S. V. Dorozhkin, Biomatter 1 (2), 121 (2011).

    Article  Google Scholar 

  4. T. J. Webster, C. Ergun, R.H. Doremus, et al., Biomaterials 22, 1327 (2001).

    Article  CAS  Google Scholar 

  5. A. M. Smolegovskii, History of Phosphate Crystal Chemistry (Nauka, Moscow, 1986) [in Russian].

    Google Scholar 

  6. J. C. Elliot, Structure, Chemistry of Apatites and Other Calcium Orthophosphates (Elsevier, Amsterdam, 1994).

    Google Scholar 

  7. R. Z. LeGerros, Adv. Dent. Res. 2, 164 (1988).

    Article  Google Scholar 

  8. S. V. Dorozhkin, Mater. Sci. Eng. C 33, 3085 (2013).

    Article  CAS  Google Scholar 

  9. S. V. Dorozhkin, Int. J. Chem. Mater. Sci. 1 (6), 105 (2013).

    Google Scholar 

  10. Advances in Induction and Microwave Heating of Mineral and Organic Materials, Ed. by S. Grundas (InTech, Croatia, 2013).

  11. S. Das, A. K. Mukhopadhyay, S. Datta, et al., Bull. Mater. Sci. 32 (1), 1 (2009).

    Article  CAS  Google Scholar 

  12. N. A. Zakharov, M. Yu. Sentsov, and V. T. Kalinnikov, Russ. J. Inorg. Chem. 58, 1412 (2013).

    Article  CAS  Google Scholar 

  13. G. Schwarzenbach and H. Flaschka, Die Komplexometrische Titration (Ferdinand Enke, Stuttgart, 1965).

    Google Scholar 

  14. S. V. Dorozhkin, Biomatter 1 (2), 121 (2011).

    Article  Google Scholar 

Download references

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, 119991, Russia

    N. A. Zakharov, M. Yu. Sentsov & N. T. Kuznetsov

Authors
  1. N. A. Zakharov
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  2. M. Yu. Sentsov
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  3. N. T. Kuznetsov
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Correspondence to N. A. Zakharov.

Additional information

Original Russian Text © N.A. Zakharov, M.Yu. Sentsov, N.T. Kuznetsov, 2017, published in Zhurnal Neorganicheskoi Khimii, 2017, Vol. 62, No. 1, pp. 26–31.

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Zakharov, N.A., Sentsov, M.Y. & Kuznetsov, N.T. Effect of microwave exposure on the morphology of calcium hydroxyapatite nanocrystals synthesized from aqueous solutions. Russ. J. Inorg. Chem. 62, 22–26 (2017). https://doi.org/10.1134/S0036023617010247

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  • DOI: https://doi.org/10.1134/S0036023617010247

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