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Synthesis of Pb8Pr2(GeO4)4(VO4)2 and refinement of its crystal structure

  • Synthesis and Properties of Inorganic Compounds
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Abstract

The conditions of synthesis of lead praseodymium vanadatogermanate Pb8Pr2(GeO4)4(VO4)2 with an apatite structure were determined by X-ray powder diffraction. The elemental composition and homogeneity of the synthesized sample were verified by scanning electron microscopy. The crystal structure was refined by the Rietveld method.

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Authors and Affiliations

  1. Donetsk National University, ul. Universitetskaya 24, Donetsk, 83001, Ukraine

    N. V. Yablochkova

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  1. N. V. Yablochkova
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Original Russian Text © N.V. Yablochkova, 2013, published in Zhurnal Neorganicheskoi Khimii, 2013, Vol. 58, No. 7, pp. 871–874.

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Yablochkova, N.V. Synthesis of Pb8Pr2(GeO4)4(VO4)2 and refinement of its crystal structure. Russ. J. Inorg. Chem. 58, 769–772 (2013). https://doi.org/10.1134/S0036023613070255

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  • DOI: https://doi.org/10.1134/S0036023613070255

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