Skip to main content
SpringerLink
Log in

Ultra-high-Silica ZSM-5 Zeolites: Synthesis and Properties

  • Synthesis and Properties of Inorganic Compounds
  • Published:
Russian Journal of Inorganic Chemistry Aims and scope Submit manuscript

Abstract

ZSM zeolites with silica ratios of 100–260 were synthesized with hexamethylenediamine (HMDA) as the structure former. IR spectroscopy and X-ray powder diffraction identified the products with ZSM-5 zeolites with more than 90% crystallinity. The unit cell parameters, specific surface area, and morphology were determined for zeolite samples. The composition of precursor alumina—silica gel was shown to influence the physicochemical characteristics of zeolites.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. V. G. Stepanov and K. G. Ione, Katal. Prom-ti, No. 2, 49 (2003).

  2. O. V. Klimov, O. V. Kikhtyanin, D. G. Aksenov, et al., KhTTM, No. 5, 20 (2005).

  3. L. M. Velichkina, L. L. Korobitsyna, and A. V. Vosmerikov, Neftepererab. Neftekhim., No. 10, 32 (2005).

  4. O. N. Kashin, A. D. Ermolenko, T. G. Firsova, and M. G. Rudin, Neftepererab. Neftekhim., No. 5, 32 (2005).

  5. Patent FRG No. 2831334 (1980).

  6. B. K. Nefedov, KhTTM, No. 3, 2 (1992).

  7. Analyses and Tests of Petroleum and Petrochemicals, Ed. by E. M. Nikonorov (Nauka, Moscow, 1986) [in Russian].

  8. P. A. Jacobs, E. G. Derouane, and J. Weitkamp, J. Chem. Soc., Chem. Commun., No. 12, 591 (1981).

  9. D. Breck, Zeolite Moleculr Sieves (Wiley, New York, 1974; Mir, Moscow, 1976).

    Google Scholar 

  10. A. V. Vosmerikov, L. L. Korobitsyna, N. V. Arbuzova, and V. I. Radomskaya, Zh. Neorg. Khim. 47(11), 1873 (2002) [Russ. J. Inorg. Chem. 47 (11), 1722 (2002)].

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Petrochemistry, Siberian Branch, Russian Academy of Sciences, Akademicheskii pr. 3, Tomsk, 634055, Russia

    L. L. Korobitsyna, L. M. Velichkina, A. V. Vosmerikov & N. V. Ryabova

  2. Institute of Geology and Nature Management, Far-East Division, Russian Academy of Sciences, ul. B. Khmelnitskogo 2, Blagoveshchensk, 67500, Russia

    V. I. Radomskaya

  3. Amur State University, Ignat’evskoe sh. 21, Blagoveshchensk, 675027, Russia

    E. S. Astapova & O. A. Agapyatova

Authors
  1. L. L. Korobitsyna
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. L. M. Velichkina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. V. Vosmerikov
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. I. Radomskaya
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. E. S. Astapova
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. N. V. Ryabova
    View author publications

    You can also search for this author in PubMed Google Scholar

  7. O. A. Agapyatova
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Korobitsyna, L.L., Velichkina, L.M., Vosmerikov, A.V. et al. Ultra-high-Silica ZSM-5 Zeolites: Synthesis and Properties. Russ. J. Inorg. Chem. 53, 169–173 (2008). https://doi.org/10.1134/S0036023608020034

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0036023608020034

Keywords

Search

Navigation