Abstract
This work has studied the effect of severe plastic deformation performed by high pressure torsion at 8 GPa and room temperature on the crystallographic structure, microhardness, and magnetic susceptibility of the ferromagnetic Ni47Mn42In11 alloy. The size of structural elements decreases, whereas the fraction of a ductile fracture constituent and the microhardness increase with increasing true strain. Severe plastic deformation performed by high pressure torsion results in phase transformation. No modulated martensite is observed in the structure after deformation.
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REFERENCES
Y. Sutou, Y. Imano, N. Koeda, T. Omori, R. Kainuma, K. Ishida, and K. Oikawa, “Magnetic and martensitic transformations of NiMnX (X = In, Sn, Sb) ferromagnetic shape memory alloys,” Appl. Phys. Lett. 85, 4358–4360 (2004).
Yu. V. Kaletina and E. G. Gerasimov, “Martensitic transformations and magnetic properties of nonstoichiometric alloys of the Ni–Mn–In system,” Phys. Solid State 56, 1634–1638 (2014).
V. D. Buchelnikov and V. V. Sokolovskiy, “Magnetocaloric effect in Ni–Mn–X (X = Ga, In, Sn, Sb) Heusler alloys,” Phys. Met. Metallogr. 112, 633–665 (2011).
Yu. V. Kaletina, V. M. Schastlivtsev, and E. A. Fokina, “Phase transformations and properties of the Ni–Mn–In Heusler alloy,” Tech. Phys. Lett. 39, 529–532 (2013).
Yu. V. Kaletina, E. G. Gerasimov, V. M. Schastlivtsev, E. A. Fokina, and P. B. Terent’ev, “Magnetic-field-induced martensitic transformations in Ni47 – xMn42 + xIn11 (0 ≤ x ≤ 2),” Phys. Met. Metallogr. 114, 838–844 (2013).
N. I. Kourov, A. V. Korolev, and V. G. Pushin, “Effect of plastic deformation by torsion on the heat capacity of the Ni50.5Ti49.5 alloy,” Phys. Solid State 54, 883–885 (2012).
N. I. Kourov, V. G. Pushin, A. V. Korolev, V. A. Kazantsev, E. B. Marchenkova, and A. N. Uksusnikov, “Effect of severe plastic deformation on the structure and properties of the Ni2.16Mn0.84Ga alloy,” Phys. Met. Metallogr. 103, 270–277 (2007).
N. I. Kourov, A. V. Korolev, V. G. Pushin, and E. V. Marchenkova, “Effect of the megaplastic torsion deformation on the heat capacity of the Ni2MnGa alloy,” Phys. Solid State 54, 2128–2131 (2012).
N. I. Kourov, V. G. Pushin, A. V. Korolev, V. V. Marchenkov, E. B. Marchenkova, and V. A. Kazantsev, “Effect of severe plastic deformation by torsion on the properties and structure of the Ni54Mn21Ga25 and Ni54Mn20Fe1Ga25 alloys,” Phys. Solid State 53, 91–99 (2011).
I. I. Musabirov, I. M. Safarov, R. R. Mulyukov, I. Z. Sharipov, V. V. Koledov, “The development of martensitic transformation in the polycrystalline Ni52Mn24Ga24 alloy as a result of severe plastic deformation and subsequent heat treatment,” Pis’ma Mater. 4, 265–268 (2014).
I. I. Musabirov, I. M. Safarov, I. Z. Sharipov, R. R. Mulyukov, A. V. Mashirov, V. V. Koledov, “Influence of deformation-heat treatment of a polycrystalline Heusler alloy Ni2.19Fe0.04Mn0.77Ga on the evolution of the microstructure and development of martensitic transformation,” Zh. Radioelektr. 1, 1–14 (2015).
I. I. Musabirov, I. M. Safarov, R. M. Galeev, D. D. Afonichev, V. V. Koledov, A. I. Rudskoi, and R. R. Mulyukov, “Plastic deformation of the Ni–Mn–Ga alloy by multiple isothernal forging,” Mater. Phys. Mech. 33, 124–136 (2017).
T. I. Chashchukhina, L. M. Voronova, M. V. Degtyarev, and D. K. Pokryshkina, “Deformation and dynamic recrystallization in copper at different deformation rates in Bridgman anvils,” Phys. Met. Metallogr. 111, 304–313 (2011).
Yu. V. Kaletina, I. G. Kabanova, N. Yu. Frolova, V. M. Gundyrev, and A. Yu. Kaletin, “Crystallographic specific features of the martensitic structure of Ni47Mn42In11 alloy,” Phys. Solid State 59, 2008–2015 (2017).
Yu. V. Kaletina, N. Yu. Frolova, V. M. Gundyrev, and A. Yu. Kaletin, “Phase transformations and structure of Ni–Mn–In alloys with varying ratio Ni/Mn,” Phys. Solid State 58, 1663–1670 (2016).
Yu. V. Kaletina, I. G. Kabanova, N. Yu. Frolova and A. Yu. Kaletin, “Crystal structure peculiarities of martensite in the Ni47Mn42In11 alloy that underwent forward and reverse phase transformations,” Phys. Met. Metallogr. 119, 383–387 (2018).
J. Ren, H. Li, S. Feng, Q. Zhai, J. Fu, Z. Luo, and H. Zheng, “Giant magnetocaloric effect in a Heusler Mn50Ni40In10 unidirectional crystal,” Intermetallics 65, 10–14 (2015).
ACKNOWLEDGMENTS
This work was performed within the state assignment of FASO of Russia, the cooperative laboratory of the Ural Federal University n.a. the First President of Russia B.N.Yeltsin and the Mikheev Institute of Metal Physics of the Ural Branch of the Russian Academy of Sciences (theme “Structure” no. AAAA-A18-118020190116-6 ) and supported in part by the Russian Foundation for Basic Research (project no. 16-03-00043). We thank N.V. Nikolaeva for the scanning microscopy examination and E.G. Gerasimov for magnetic measurements and his participation in discussions of the experimental results.
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Translated by T. Gapontseva
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Kaletina, Y.V., Greshnova, E.D., Kaletin, A.Y. et al. Structure and Properties of Ni47Mn42In11 Alloy after Severe Plastic Deformation. Phys. Metals Metallogr. 120, 171–176 (2019). https://doi.org/10.1134/S0031918X19020078
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DOI: https://doi.org/10.1134/S0031918X19020078