Abstract
The history of the research of anomalous diffuse scattering by perfect single crystals has been briefly described. Some traditional techniques for recording the diffuse scattering have been considered. The mono-Laue experiment has been considered in detail. A series of mono-Laue measurements on single-crystal cobalt (hcp structure) has been carried out at room temperature. The results are in a good agreement with theoretical calculations. The principal possibility of these measurements under laboratory conditions has been shown. The possible use of diffuse scattering measurements in the study of structural phase transitions in metals has been substantiated.
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References
W. Friedrich, P. Knipping, and M. Laue, “Interferenzerscheinungen bei Rontgenstrahlen,” Ann. Phys. (New York) 346 (10), 971–988 (1913).
W. L. Bragg, “The Structure of some crystals as indicated by their diffraction of X-rays,” Proc. R. Soc. A89, 248–277 (1913).
M. Laue, Rontgenstrahlinterferenz und Mischkristalle, Ann. Phys 361, 497–506 (1918).
K. Lonsdale and H. Smith, “An experimental study of diffuse X-ray reflexion by single crystals,” Proc. R. Soc. London, Ser. A 179, 8–50 (1941).
K. Lonsdale, “X-ray study of crystal dynamics: An historical and critical survey of experiment and theory,” Proc. Phys. Soc. 54 (304), 314–353 (1942).
R. Comès, F. Denoyer, L. Deschamps, and M. Lambert, “Critical anisotropic fluctuations at the 184 K transition of KMnF3 single crystal,” Phys. Lett. A. 32, 65–66 (1971).
F. Denoyer, R. Comès, and M. Lambert, “Anisotropic critical X-ray diffuse scattering from NaNbO3 crystals,” Solid. State Commun. 8, 1979–1981 (1970).
K. Koto and H. Schultz, “X-ray diffuse scattering from wurtzite-type compounds,” Acta Crystallogr. A 35, 971–974 (1979).
F. A. Kassan-Ogly, V. E. Naish, and Yu. E. Turkhan, “Theory of structural transformations in the compounds of the A15 type,” Fiz. Met. Metalloved. 65, 645–657 (1988).
F. A. Kassan-Ogly, V. E. Naish, and I. V. Sagaradze, “Problems of the interpretation ofX-ray diffraction patterns of diffuse scattering,” Fiz. Met. Metalloved. 67, 451–461 (1989).
R. Comès, M. Lambert, and A. Guinier, “Desordre lineaire dans les cristaux (cas du silicium, du quartz et de perovskites ferroelectriques),” Acta Crystallogr. A 26, 244–254 (1970).
F. A. Kassan-Ogly and V. E. Naish, “The immanent chaotization of crystal structures and the resulting diffuse scattering. II. Crystallochemical conditions of per ovskite chaotization,” Acta Crystallogr. B 42, 307–313 (1986).
F. A. Kassan-Ogly and V. E. Naish, “The immanent chaotization of crystal structures and the resulting diffuse scattering. III. Diffuse scattering in perovskites with one-dimensional movable objects (“shifting”),” Acta Crystallogr. B 42, 314–324 (1986).
F. A. Kassan-Ogly and V. E. Naish, “The immanent chaotization of crystal structures and the resulting diffuse scattering. IV. Diffuse Scattering in Perovskites with Two-Dimensional Movable Objects (“Tilting”),” Acta Crystallogr. B 42, 325–335 (1986).
Ryabchikov, D.I. and Ryabuchin, V.A., Analytical Chemistry of Rare-Earth Elements and Yttrium (Nauka, Moscow, 1966 [in Russian].
F. A. Kassan-Ogly, V. E. Naish, and I. V. Sagaradze, “Diffuse scattering in metals with a bcc lattice and the crystallogeomentry of martensitic phase transitions of the bcc–fcc and bcc–hcp types,” Fiz. Met. Metalloved. 65 (3), 481–491 (1988).
F. A. Kassan-Ogly, V. E. Arkhipov, and A. E. Shestakov, “Phase Transitions in Crystals with a BCC Structure,” Phys. Met. Metallogr. 109, 568–584 (2010).
G. Honjo, S. Kodera, and N. Kitamura, “Diffuse streak diffraction patterns from single crystals. I. General discussion and aspects of electron diffraction diffuse streak patterns,” J. Phys. Soc. Jpn. 19, 351–367 (1964).
K. Komatsu and K. Teramoto, “Diffuse streak patterns from various crystals in X-ray and electron diffraction,” J. Phys. Soc. Jpn. 21, 1152–1159 (1966).
A. E. van Arkel, Reine Metalle (Berlin, Springer, 1936).
O. S. Edwards and H. Lipson, “Imperfections in the structure of cobalt. I. Experimental work and proposed structure,” Proc. R. Soc. London, Ser. A 180, 268–277 (1942).
Yu. V. Khlebnikova, D. P. Rodionov, V. A. Sazonova, T. I. Tabatchikova, O. V. Antonova, Yu. E. Turkhan, and V. A. Kazantsev, “Study of the structure of cobalt single crystals during the β → a transformation,” Phys. Met. Metallogr. 103, 609–618 (2007).
Yu. V. Khlebnikova, T. I. Tabatchikova, D. P. Rodionov, and V. A. Sazonova, “Crystallographic aspects of structure formation under the β→a transformation in oriented cobalt single crystals,” Bull. Russ. Acad. Sci.: Phys. 73, 1207–1210 (2009).
V. M. Schastlivtsev, Yu. V. Khlebnikova, T. I. Tabatchikova, D. P. Rodionov, and V. A. Sazonova, “Formation of a structure in cobalt single crystals at the beta–alpha transformation,” Dokl. Phys. 54, 21–24 (2009).
C. -S. Yoo, P. Söderlind, and H. Cynn, “The phase diagram of cobalt at high pressure and temperature: The stability of γ(fcc)-cobalt and new e'(dhcp)-cobalt,” J. Phys.: Condens. Matter. 10, L311–L318 (1998).
S. V. Vonsovskii, Magnetism (Nauka, Moscow, 1071) [in Russian].
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Original Russian Text © A.E. Shestakov, F.A. Kassan-Ogly, Yu.E. Turkhan, 2018, published in Fizika Metallov i Metallovedenie, 2018, Vol. 119, No. 3, pp. 243–253.
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Shestakov, A.E., Kassan-Ogly, F.A. & Turkhan, Y.E. Diffuse Scattering from Single Crystal Cobalt. Phys. Metals Metallogr. 119, 229–240 (2018). https://doi.org/10.1134/S0031918X18030122
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DOI: https://doi.org/10.1134/S0031918X18030122