Abstract
The main mechanisms of grain growth upon low-temperature recrystallization of pure nickel (99.98%) with structures of various types formed upon deformation in Bridgman anvils have been studied. A decrease in the amount of the stored energy of deformation at the stage of submicrocrystalline (SMC) structure has been revealed using the method of differential scanning calorimetry. The isothermal annealings with durations of up to 64 h made it possible to show that the low-temperature recrystallization in both the mixed and SMC structures is developed via the growth of separate centers that are formed during deformation. As a result, no homogeneous submicrograin structure is formed in nickel upon low-temperature recrystallization.
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References
N. I. Noskova and R. R. Mulyukov, Submicrocrystalline and Nanocrystalline Metals and Alloys (Ural. Otd. Ross. Akad. Nauk, Ekaterinburg, 2003) [in Russian].
M. V. Degtyarev, L. M. Voronova, V. V. Gubernatorov, and T. I. Chashchukhina, “On the thermal stability of microcrystalline structure in single-phase metallic materials,” Dokl.-Phys. 47, 647–650 (2002).
L. M. Voronova, M. V. Degtyarev, and T. I. Chashchukhina, “Recrystallization of the ultradispersed structure of pure iron formed at different stages of the deformation-induced strain hardening,” Phys. Met. Metallogr. 104, 262–273 (2007).
N. A. Smirnova, V. I. Levit, V. P. Pilyugin, R. I. Kuznetsov, L. S. Davydova, and V. A. Sazonova, “Evolution of structure of fcc single crystals subjected to large plastic deformation,” Phys. Met. Metallogr. 61, 127–134 (1986).
V. P. Pilyugin, T. M. Gapontseva, T. I. Chashchukhina, L. M. Voronova, L. I. Shchinova, and M. V. Degtyarev, “Evolution of the structure and hardness of nickel upon cold and low-temperature deformation under pressure,” Phys. Met. Metallogr. 105, 409–419 (2008).
A. Belyakov, K. Tsuzaki, H. Miura, and T. Sakai, “Effect of initial microstructures on grain refinement in a stainless steel by large strain deformation,” Acta Mater. 51, 847–861 (2003).
N. A. Smirnova, V. I. Levit, V. P. Pilyugin, R. I. Kuznetsov, and M. V. Degtyarev, “The low temperature recrystallization of nickel and copper,” Phys. Met. Metallogr. 62, 140–144 (1986).
V. M. Bykov, V. A. Likhachev, Yu. A. Nikonov, L. L. Serbina, and L. I. Shibalova, “Fragmentation and dynamic recrystallization of copper at large and very large plastic deformations,” Fiz. Met. Metalloved. 45, 163–169 (1978).
T. I. Chashchukhina, M. V. Degtyarev, M. Yu. Romanova, and L. M. Voronova, “Dynamic recrystallization in copper deformed by shear under pressure,” Phys. Met. Metallogr. 98, 639–647 (2004).
I. A. Ditenberg, A. N. Tyumentsev, A. V. Korznikov, and E. A. Korznikova, “Microstructural evolution of nickel under high-pressure torsion,” Phys. Mezomech. 3, 239–247 (2013).
M. A. Shtremel’, Strength of Alloys. Ch. 1. Lattice Defects (Metallurgiya, Moscow, 1982) [in Russian].
A. V. Korznikov, G. F. Korznikova, M. M. Myshlyaev, R. Z. Valiev, D. Salimonenko, and O. Dimitrov, “Evolution of nanocrystalline Ni structure during heating,” Phys. Met. Metallogr. 84, 413–417 (1997).
H. W. Zhang, X. Huang, R. Pippan, and N. Hansen, “Thermal behavior of Ni (99.967% and 99.5% purity) deformed to an ultra-high strain by high pressure torsion,” Acta Mater. 58, 1698–1707 (2010).
A. A. Nazarova, R. R. Mulyukov, V. V. Rubanik, Yu. V. Tsarenko, and A. A. Nazarov, “Effect of ultrasonic treatment on the structure and properties of ultrafine-grained nickel,” Phys. Met. Metallogr. 110, 574–581 (2010).
V. V. Popov, E. N. Popova, D. D. Kuznetsov, A. V. Stolbovskii, and V. P. Pilyugin, “Thermal stability of nickel structure obtained by high-pressure torsion in liquid nitrogen,” Phys. Met. Metallogr. 115, 682–691 (2014).
M. V. Degtyarev, T. I. Chashchukhina, L. M. Voronova, A. M. Patselov, and V. P. Pilyugin, “Influence of the relaxation processes on the structure formation in pure metals and alloys under high-pressure deformation,” Acta Mater. 55, 6039–6050 (2007).
V. I. Trefilov, V. F. Moiseev, E. P. Pechkovskii, I. D. Gornaya, and A. D. Vasil’ev, Stain Hardening and Fracture of Polycrystalline Metals (Naukova Dumka, Kiev, 1987) [in Russian].
Saltykov, S. A., Quantitative Metallography (Metallurgiya, Moscow, 1970) [In Russian].
A. P. Zhilyaev, G. V. Nurislamova, R. Z. Valiev, S. Lee, and T. G. Langdon, “Microhardness and microstructural evolution in pure nickel during high-pressure torsion,” Scr. Mater. 44, 2753–2758 (2001).
S. S. Gorelik, Recrystallization of Metals and Alloys (Metallurgiya, Moscow, 1978) [in Russian].
M. V. Degtyarev, L. M. Voronova, and T. I. Chashchukhina, “Grain growth upon annealing of Armco iron with various ultrafine-grained structures produced by high-pressure torsion deformation,” Phys. Met. Metallogr. 99, 276–285 (2005).
M. V. Degtyarev, T. I. Chashchukhina, L. M. Voronova, L. S. Davydova, and V. P. Pilyugin, “Deformation strengthening and structure of structural steel upon shear under pressure,” Phys. Met. Metallogr. 90, 604–611 (2000).
L. M. Voronova, M. V. Degtyarev, and T. I. Chashchukhina, “Thermal stability of submicrocrystalline structure in 4Kh14N14V2M steel,” Phys. Met. Metallogr. 109, 135–141 (2010).
V. Yu. Novikov, Secondary Recrystallization (Metallurgiya, Moscow, 1990) [in Russian].
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Original Russian Text © Yu.G. Krasnoperova, L.M. Voronova, M.V. Degtyarev, T.I. Chashchukhina, N.N. Resnina, 2015, published in Fizika Metallov i Metallovedenie, 2015, Vol. 116, No. 1, pp. 83–90.
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Krasnoperova, Y.G., Voronova, L.M., Degtyarev, M.V. et al. Recrystallization of nickel upon heating below the temperature of thermoactivated nucleation. Phys. Metals Metallogr. 116, 79–86 (2015). https://doi.org/10.1134/S0031918X15010081
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DOI: https://doi.org/10.1134/S0031918X15010081