Abstract
The effect of heat treatment and partial oxidation of an Fe50Mn50 layer on the structure and magnetic properties of exchange-coupled Fe20Ni80/Fe50Mn50 layers has been investigated. The behavior of the exchange-bias field and coercive force depending on the temperature of annealing upon heat treatment in a vacuum or in an oxygen-containing gas mixture has been studied. It has been shown that, by adjusting the parameters of annealing in the gas mixture, it is possible to increase the field of switching of the exchange-coupled Fe20Ni80/Fe50Mn50 layers.
Similar content being viewed by others
References
W. H. Meiklejohn and C. P. Bean, “New magnetic anisotropy,” Phys. Rev. 102, 1413–1414 (1956).
A. A. Glazer, R. I. Tagirov, A. P. Potapov, and Ya. S. Shur, “Exchange anisotropy in thin magnetic films,” Fiz. Tverd. Tela 8, 3022–3031 (1966).
A. Yelon, “Interactions in multilayer magnetic films,” in Physics of Thin Films, Ed. by M. H. Francombe and R. W. Hoffman, (Academic, New York, 1971), vol. 6.
C. Tang, “Magnetics of small magnetoresistive sensors,” J. Appl. Phys. 55, 2226–2231 (1984).
B. Dieny, V. S. Speriosu, S. S. P. Parkin, B. A. Gurney, D. R. Wilhoit, and D. Mauri, “Giant magnetoresistance in soft ferromagnetic multilayers,” Phys. Rev. B: Condens. Matter 41, 1297–1300 (1991).
J. Nogués, J. Sort, V. Langlais, V. Skumryev, S. Surinach, J. S. Munoz, and M. D. Baro, “Exchange bias in nanostructures,” Phys. Rep. 422, 65–117 (2005).
N. J. Oliveira, J. L. Ferreira, J. Pinheiro, A. M. Fernandes, O. Redon, S. X. Li, P. Berge, T. S. Plaskett, and P. P. Freitas, “Improvement of thermal stability and magnetoresistance recovery of Tb25Co75 biased spin-valve heads,” J. Appl. Phys. 81, 4903–4905 (1997).
A. V. Svalov, V. O. Vas’kovskii, and Yu. M. Yarmoshenko, “Production and study of spin-valve structures on the basis of permalloy films,” Fiz. Met. Metalloved. 79, 53–57 (1995).
M. Xu, Z. Lu, T. Yang, C. Liu, S. Cui, Z. Mai, W. Lai, Q. Jia, and W. Zheng, “Relation between microstructures and magnetic properties upon annealing in Fe50Mn50/Ni80Fe20 films,” J. Appl. Phys. 92, 2052–2057 (2002).
M. Koguchi, H. Kakibayashi, and R. Nakatani, “Observation of Fe-Mn oxidation process using specimen transfer chamber and ultrahigh-vacuum transmission electron microscope,” Jpn. J. Appl. Phys. 32, 4814–4818 (1993).
H. Lefakis, T. C. Huang, and P. Alexopoulos, “Surfaceoxidation-induced phase separation in FeMn thin films,” J. Appl. Phys. 64, 5667–5669 (1988).
S. L. Cohen, M. A. Russak, J. M. Baker, T. R. McGuire, G. J. Scilla, and S. M. Rossnagel, “Characterization of the surface oxidation and magnetic properties of MnFe thin films,” J. Vac. Sci. Technol. A 6, 918–923 (1988).
P. A. Savin, V. N. Lepalovskii, A. N. Gor’kovenko, and V. O. Vas’kovskii, “Exchange displacement in Fe19Ni81/Fe50Mn50 films,” Proc. 22nd Int. Conf. “New in Magnetism and Magnetic Materials” (NMMM XXII)), Astrakhan’, 2012, pp. 549–550.
H. Umbayashi and Y. Ishikawa, “Antiferromagnetism of γ Fe-Mn alloys,” J. Phys. Soc. Jpn. 21, 1281–1294 (1966).
V. N. Lepalovskii, “Magnetoresistance of and hysteresis properties of FeCoNi films with varied microstructure,” Candidate Sci. (Math.-Phys.) Dissertation (Ural. Gos. Univ., Ekaterinburg, 2002).
G. H. Yu, M. H. Li, J. Teng, F. W. Zhu, W. and Y. Lai, “Interface reactions in Ta/Ni81Fe19/Ta structures and their influence on magnetic properties,” Thin Solid Films 484, 208–214 (2005).
A. Choukh, “Effect of interface on exchange coupling in NiFe/FeMn system,” IEEE Trans. Magn. 33, 3676–3678 (1997).
M. Xu, Z. Lu, T. Yang, C. Liu, S. Cui, Z. Mai, W. Lai, Q. Jia, and W. Zheng, “Relation between microstructures and magnetic properties upon annealing in Fe50Mn50/Ni80Fe20 films,” J. Appl. Phys. 92, 2052–2057 (2002).
K.-Y. Kim, H.-C. Choi, J.-H. Shim, D.-H. Kim, C.-Y. You, and J.-S. Lee, “Ferromagnetic resonance study of annealed NiFe/FeMn/CoFe trilayers,” IEEE Trans. Magn. 45, 2766–2769 (2009).
M. F. Toney, C. Tsang, and J. K. Howard, “Thermal annealing study of exchange-biased NiFe-FeMn films,” J. Appl. Phys. 70, 6227–6229 (1991).
J. H. Lee, H. D. Jeong, C. S. Yoon, C. K. Kim, B.G. Park, and T. D. Lee, “Interdiffusion in antiferromagnetic/ferromagnetic exchange coupled NiFe/IrMn/CoFe multilayer,” J. Appl. Phys. 91, 1431–1435 (2002).
W. E. Wallace and M. Q. Huang, “Enhanced Fe moment in nitrogen martensite and Fe16N2,” J. Appl. Phys. 76, 6648–6652 (1994).
P. Bezdička, A. Kláriková, I. Paseka, and K. Závěta, “Magnetic properties of α′-FeNx and α″-Fe16N2 nitrides,” J. Alloys Compd. 274, 10–17 (1998).
X. P. Feng, W. B. Mi, and H. L. Bai, “Polycrystalline iron nitride films fabricated by reactive facing-target sputtering: Structure, magnetic and electrical transport properties,” J. Appl. Phys. 110, 053911 (2011).
S. T. Halloran, F. C. S. Silva, H. Z. Fardi, and D. P. Pappas, “Permanent-magnet-free stabilization and sensitivity tailoring of magnetoresistive field sensors,” J. Appl. Phys. 102, 033904 (2007).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © P.A. Savin, V.N. Lepalovskij, A.V. Svalov, V.O. Vas’kovskiy, G.V. Kurlyandskaya, 2014, published in Fizika Metallov i Metallovedenie, 2014, Vol. 115, No. 9, pp. 913–920.
Rights and permissions
About this article
Cite this article
Savin, P.A., Lepalovskij, V.N., Svalov, A.V. et al. Effect of phase separation in an Fe20Ni80/Fe50Mn50 structure with exchange coupling. Phys. Metals Metallogr. 115, 856–863 (2014). https://doi.org/10.1134/S0031918X14070096
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0031918X14070096