Abstract
Structure of a metastable austenitic invar alloy Fe-32% Ni preliminarily quenched for martensite and subjected to α → γ transformation using slow heating to various temperatures (430–500°C) with the formation of variously oriented nanocrystalline lamellar austenite, which was subjected to an additional annealing at 280°C (below the calculated temperature of ordering of the γ phase), has been studied electron-microscopically. An electron diffraction analysis revealed the presence of an L10 superstructure in the disperse nickel-enriched nanocrystalline γ phase both after annealing at 280°C and in the unannealed alloy immediately after α → γ transformation upon slow heating to 430°C.
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K. A. Malyshev, V. V. Sagaradze, I. P. Sorokin, A. I. Uvarov, V. A. Teplov, and N. D. Zemtsova, Transformation-Induced Hardening of Iron-Nickel-Based Austenitic Steels (Nauka, Moscow, 1982) [in Russian].
V. V. Sagaradze and A. I. Uvarov, Strengthening Austenitic Steels (Nauka, Moscow, 1989) [in Russian].
V. V. Sagaradze, “The Properties of Fe-Ni FCC Alloys Having a Nanostructure Produced by Deformation, Irradiation and Cyclic Phase Transformation,” Nanostruct. Mater. Sci. Technol. 50(12), 243–262 (1998).
V. V. Sagaradze and V. A. Shabashov, “Origin of Active Low-Temperature Redistribution of Nickel in Iron-Nickel Alloys,” Fiz. Met. Metalloved. 57, 1166–1171 (1984).
I. G. Kabanova and V. V. Sagaradze, “On the Habit of FCC Phase Formed upon Heating in Crystals of Martensite and Polyhedral Ferrite with a BCC Lattice,” Fiz. Met. Metalloved. 58, 522–531 (1984).
I. G. Kabanova and V. V. Sagaradze, “Statistical Analysis of Mutual Misorientations of Austenite (Martensite) Crystals after γ → α → γ (α → γ → α) Martensitic Transformations,” Phys. Met. Metallogr. 88(2), 143–151 (1999).
J. F. Albertsen, “Tetragonal Lattice of Tetrataenite (Ordered Fe-Ni, 50-50) from 4 Meteorites,” Phys. Scr. 23, 301–306 (1981).
K. B. Reuter, D. B. Williams, and J. I. Goldstein, “Determination of the Fe-Ni Phase Diagram below 400°C,” Metall. Trans. A 20, 719–725 (1989).
J. Yang and J. I. Golstein, “An Improved Model to Determine the Cooling Rates of Mesosiderites and Iron Meteorites,” http://www.lpi.usra.edu/meetings/lpsc2003/pdf/1156.pdf
V. G. Myagkov, O. Yu. Bayukov, L. E. Bykova, V. S. Zhi- galov, and G. N. Bondarenko, “Solid-State Synthesis in Ni/Fe/MgO(001) Epitaxial Thin Films,” JETP Lett. 80, 487–490 (2004).
A. Chamberod, J. Laugier, and J. M. Penisson, “Electron Irradiation Effects on Iron-Nickel Invar Alloys,” J. Magn. Magn. Mater. 10, 139–144 (1979).
A. I. Deryagin, V. A. Zavalishin, V. V. Sagaradze, A. R. Kuznetsov, V. A. Ivchenko, N. F. Vil’danova, and B. M. Efros, “Effect of Composition and Temperature on the Redistribution of Alloying Elements in Fe-Cr-Ni Alloys during Cold Deformation,” Phys. Met. Metallogr. 106, 291–301 (2008).
J. F. Albertsen, H. P. Nielsen, and V. F. Buchwald, “On the Fine Structure of Meteoritical Taenite/Tetrataenite and Its Interpretation,” Phys. Scr. 27, 314–320 (1983).
T. J. Headley and J. A. Brooks, “A New BCC-FCC Orientation Relationship Observed between Ferrite and Austenite in Solidification Structures of Steels,” Metall. Mater. Trans. A 33, 5–15 (2002).
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Original Russian Text © I.G. Kabanova, V.V. Sagaradze, N.V. Kataeva, 2011, published in Fizika Metallov i Metallovedenie, 2011, Vol. 112, No. 3, pp. 285–294.
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Kabanova, I.G., Sagaradze, V.V. & Kataeva, N.V. Formation of an L10 superstructure in austenite upon the α → γ transformation in the invar alloy Fe-32% Ni. Phys. Metals Metallogr. 112, 267–276 (2011). https://doi.org/10.1134/S0031918X11030197
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DOI: https://doi.org/10.1134/S0031918X11030197