Abstract
We present a concept design of the CCU SKIF–NSU Experimental Station 1-7 “Basic methods of synchrotron diagnostics for educational, research, and innovative activities of students” for improving the efficiency of the educational process and helping the NSU students to solve research problems using the capabilities of a modern synchrotron radiation source. Several research methods are planned to be jointly implemented at the Experimental Station 1-7: powder and single-crystal X-ray diffraction, X-ray absorption spectroscopy, and X-ray fluorescence analysis. This research complex will not only allow solving a wide range of scientific problems in various fields of science such as physics, biology, chemistry, geology, archeology and medicine, but will also become an essential element of the practical education of scientific and technical stuff for the synchrotron research.
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REFERENCES
A. Lanzirotti. Focus on Synchrotron Education Initiatives. Synchrotron Radiat. News, 2013, 26(1), 2-4. https://doi.org/10.1080/08940886.2013.753768
T. L. Walker and R. I. R. Blyth. Inquiry for Inspiration: The Students on the Beamlines Program at the Canadian Light Source. Synchrotron Radiat. News, 2013, 26(1), 21-24. https://doi.org/10.1080/08940886.2013.753778
A. Lanzirotti, S. Bronson, L. Miller, and K. Nasta. Using the NSLS for Introducing Synchrotrons into the Classroom (InSynC). Synchrotron Radiat. News, 2013, 26(1), 30-34. https://doi.org/10.1080/08940886.2013.753786
N. Mills. Synchrotron education down under. Synchrotron Radiat. News, 2013, 26(1), 16-20. https://doi.org/10.1080/08940886.2013.753776
F. Mosselmans. Synchrotron radiation school at diamond light source. Synchrotron Radiat. News, 2011, 24(1), 16-18. https://doi.org/10.1080/08940886.2011.550552
I. Halasz, S. A. J. Kimber, P. J. Beldon, A. M. Belenguer, F. Adams, V. Honkimäki, R. C. Nightingale, R. E. Dinnebier, and T. Friščić. In situ and real-time monitoring of mechanochemical milling reactions using synchrotron X-ray diffraction. Nat. Protoc., 2013, 8(9), 1718-1729. https://doi.org/10.1038/nprot.2013.100
T. Rathmann, H. Petersen, S. Reichle, W. Schmidt, A. P. Amrute, M. Etter, and C. Weidenthaler. In situ synchrotron X-ray diffraction studies monitoring mechanochemical reactions of hard materials: Challenges and limitations. Rev. Sci. Instrum., 2021, 92(11), 114102. https://doi.org/10.1063/5.0068627
H. Petersen, S. Reichle, S. Leiting, P. Losch, W. Kersten, T. Rathmann, J. Tseng, M. Etter, W. Schmidt, and C. Weidenthaler. In situ synchrotron X-ray diffraction studies of the mechanochemical synthesis of ZnS from its elements. Chem. - Eur. J., 2021, 27(49), 12558-12565. https://doi.org/10.1002/chem.202101260
J. Munn, P. Barnes, D. Häusermann, S. A. Axon, and J. Klinowski. In-situ studies of the hydrothermal synthesis of zeolites using synchrotron energy-dispersive X-ray diffraction. Phase Transitions, 1992, 39(1-4), 129-134. https://doi.org/10.1080/01411599208203476
J. Chen, J. Bai, H. Chen, and J. Graetz. In situ hydrothermal synthesis of LiFePO4 studied by synchrotron X-ray diffraction. J. Phys. Chem. Lett., 2011, 2(15), 1874-1878. https://doi.org/10.1021/jz2008209
M. Rehan, X. Lai, and G. M. Kale. In-situ investigation of hydrothermal synthesis of TiO2 nanoparticles using synchrotron radiation X-ray diffraction. In: Proc. 17th Int. Symp. Ind. Cryst., Maastricht, Netherlands, Sept. 14-17, 2008 / Eds. P.J. Jansens, J. Ulrich. Maastricht, Netherlands: EFCE, 2008. https://doi.org/10.13140/2.1.3512.3526
Tekhnologicheskaya infrastruktura sibirskogo koltsevogo istochnika fotonov “SKIF” (Technological Infrastructure of Synchrotron Radiation Facility SKIF) / Ed. K.I. Shefer. Novosibirsk: Boreskov Institute of Catalysis, 2022, Vol. 2: Uskoritel′nyi Kompleks (Accelerating Complex). [In Russian]
T. Tanaka. Universal representation of undulator phase errors. Phys. Rev. Accel. Beams, 2018, 21(11), 110704. https://doi.org/10.1103/physrevaccelbeams.21.110704
K. Klementiev and R. Chernikov. Powerful scriptable ray tracing package XRT. In: Advances in Computational Methods for X-Ray Optics III: Proc. SPIE, Vol. 9209, San Diego, California, USA, Sept. 5, 2014 / Eds. M. Sanchez del Rio, O. Chubar. Washington, USA: SPIE, 2014, 92090A. https://doi.org/10.1117/12.2061400
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This work was funded by the Priority 2030 Strategic Leadership Program of NSU and by the State Assignment for the Institute of Catalysis SB RAS (project AAAA-A21-121011390011-4).
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Russian Text © The Author(s), 2023, published in Zhurnal Strukturnoi Khimii, 2023, Vol. 64, No. 7, 113304.https://doi.org/10.26902/JSC_id113304
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Bulavchenko, O.A., Vinokurov, Z.S., Selyutin, A.G. et al. Concept Design of the CCU Skif–NSU Experimental Station 1-7 “Basic Methods of Synchrotron Diagnostics for Educational, Research, and Innovative Activities of Students”. J Struct Chem 64, 1329–1340 (2023). https://doi.org/10.1134/S0022476623070168
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DOI: https://doi.org/10.1134/S0022476623070168