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APPROACH TO THE STUDY OF THE DYNAMICS OF UNIT CELL PARAMETERS OF SINGLE CRYSTALS IN A WIDE TEMPERATURE RANGE ON THE EXAMPLE OF Ag0.39Li0.61GaSe2

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Abstract

We report a technique for the refinement of unit cell parameters by using external referencing for goniometer calibration, processing the 2D profile of diffraction reflection, and introducing corrections. The changes of unit cell parameters of the Ag0.39Li0.61GaSe2 single crystal is studied in the temperature range from 100 K to 480 K. As the volume of the tetragonal unit cell increases by 1%, parameter a increases by 0.6% and parameter c decreases by 0.3%.

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Funding

This work was funded by the Ministry of Science and Higher Education of the Russian Federation, project No. 121031700313-8.

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Authors and Affiliations

  1. Novosibirsk State University, Novosibirsk, Russia

    A. V. Panchenko & L. I. Isaenko

  2. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    A. S. Sukhikh & S. A. Gromilov

  3. Sobolev Institute of Geology and Mineralogy, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    L. I. Isaenko

Authors
  1. A. V. Panchenko
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  2. A. S. Sukhikh
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  3. L. I. Isaenko
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  4. S. A. Gromilov
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Corresponding author

Correspondence to S. A. Gromilov.

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The authors declare that they have no conflicts of interests.

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Russian Text © The Author(s), 2022, published in Zhurnal Strukturnoi Khimii, 2022, Vol. 63, No. 10, 99973.https://doi.org/10.26902/JSC_id99973

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Panchenko, A.V., Sukhikh, A.S., Isaenko, L.I. et al. APPROACH TO THE STUDY OF THE DYNAMICS OF UNIT CELL PARAMETERS OF SINGLE CRYSTALS IN A WIDE TEMPERATURE RANGE ON THE EXAMPLE OF Ag0.39Li0.61GaSe2. J Struct Chem 63, 1662–1669 (2022). https://doi.org/10.1134/S0022476622100122

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  • DOI: https://doi.org/10.1134/S0022476622100122

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