Abstract
A new 1D Cd(II) complex [Cd(L-pheA)(Ac)]n(1) where the L-pheA− anion stands for the chiral ligand (L-phenylalanine hydroxamic acid) is synthesized and characterized. The single crystal X-ray analysis reveals that each Cd(II) atom is coordinated by three L-pheA− ligands and two acetate anions in a distorted seven-coordinated pentagonal bipyramidal configuration. By the interactions of two N-H⋯O and one N-H⋯N hydrogen bonds a 2D supramolecular network is formed. The solid-state luminescent properties of complex 1 are observed.
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Funding
This research was supported by the Natural Science Foundation of China (grant No. 21501061), the Natural Science Foundation of Hubei Province (No. 2016CFB147), the Foundation of Hubei Educational Committee (No. D20172904), Doctoral Foundation Project of Huanggang Normal University (grant No. 2015001803), Project of Chemical Experiment Teaching Demonstration Center of Huanggang Normal University (No. zj201723, zj201722, zx201724, zx2018004).
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Supplementary material for structure 1 has been deposited with the Cambridge Crystallographic Date Centre (CCDC Nos. 1555499; deposit@ccdc.cam.ac.uk or http://www.ccdc.cam.ac.uk). These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
Text © The Author(s), 2020, published in Zhurnal Strukturnoi Khimii, 2020, Vol. 61, No. 6, pp. 925–931.
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Chen, Y.M., Xiong, X.J., Huang, L.C. et al. Synthesis, Structure and Properties of a One-Dimensional Cd(II) Complex Based on a Chiral Ligand. J Struct Chem 61, 873–879 (2020). https://doi.org/10.1134/S0022476620060050
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DOI: https://doi.org/10.1134/S0022476620060050