Abstract
A single-stage catalyst free synthesis of hydrogenated graphene was studied in the process of methane conversion in a helium plasma jet created by a plasma torch at the power up to 45 kW and the pressure of 710 Torr. The synthesis products were studied by the methods of scanning and transmission electron microscopy, thermal analysis, Raman spectroscopy, X-ray photoelectron spectroscopy, and X-ray diffraction analysis.
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References
Y. Shimazaki, M. Yamamoto, I. V. Borzenets, et al. Nat. Phys., 2015, 11, 1032.
J. Li, X. Cheng, A. Shashurin, and M. Keidar. Graphene, 2012, 1, 1.
J.–H. Lee, J. Lou, Ph. E. Loya, and E. L. Thomas. Science, 2014, 346, 1092.
X. Wang, G. Sun, P. Routh, D.–H. Kim, et al. Chem. Soc. Rev., 2014, 43, 7067.
J. Li, A. Shashurin, and M. Keidar. IEEE Trans. Plasma Sci., 2011, 11, 2366.
I. Levchenko, O. Volotskova, A. Shashurin, Y. Raitses, et al. Carbon, 2010, 15, 4570.
J. Li, A. Shashurin, M. Kundrapu, and M. Keidar. J. Visualize. Exp., 2012, 60, 3455.
M. Li, D. Liu, D. Wei, X. Song, D. Wei, and A. T. S. Wee. Adv. Sci., 2016, 3, 1600003.
E. Tatarova, J. Henriques, A. Dias, et al. J. Phys. D. Appl. Phys., 2014, 47, 385501.
A. N. Obraztsov, E. A. Obraztsova, et al. Carbon, 2007, 45(10), 2017.
R. H. Amirov, et al. Nanosyst.: Phys., Chem., Math., 2016, 7, 60.
M. B. Shavelkina, R. H. Amirov, P. P. Ivanov, and E. A. Filimonova. 16th International Workshop on Magneto–Plasma Aerodynamics. Moscow, Russia, 2017, 92.
H. Zhang, Y. Zhang, B. I. N. Wang, et al. J. Electron. Mater., 2015, 44, 80.
M. B. Shavelkina, R. H. Amirov, et al. J. Phys.. Conf., 2017, 857, 012040.
K. Norinaga, O. Deutschmann, and K. J. Hüttnger. Carbon, 2006, 44, 1790.
R. R. Nair, P. Blake, A. N. Grigorenko, et al. Science, 2008, 320, 1308.
K. S. Novoselov, V. I. Fal′ko, L. Colombo, et al. Nature, 2012, 490, 192.
M. Scheffler, D. Haberer, L. Petaccia, et al. ACS Nano, 2012, 6(12), 10590.
Hydrogen Recycling at Plasma Facing Materials. Ed. C.H. Wu. Springer Science+Business Media Dordrecht, 2000.
E. A. Denisov and T. N. Kompaniets. Technical Phys., 2001, 46, 240.
R. J. Nemanich and S. A. Solin. Phys. Rev., B., 1979, 20, 392.
K. C. Chang, C. H. Hsu, and H. I. Lu. eXPRESS Polym. Lett., 2014, 8, 243.
S.–Y. Yang, K.–H. Chang, H.–W. Tien, et al. J. Mater. Chem., 2011, 21, 2374.
A. C. Ferrari, J. C. Meyer, V. Scardaci, et al. Phys. Rev. Lett., 2006, 97, 187401.
A. C. Ferrari. Solid State Commun., 2007, 143, 47.
Y. Wu, B. Wang, Y. Ma, Y. Huang, N. Li, et al. Nano Res., 2010, 3(9), 661.
J. Son, S. Lee, S. J. Kim, B. C. Park, et al. Nature Commun., 2016, 7, 13261.
D. I. Slovetskiy. Khim. Vys. Energ., 2006, 40(2), 112.
A. I. Pushkarev and R. V. Sazonov. Khim. Vys. Energ., 2009, 43(3), 202.
J. R. Fincke, R. P. Anderson, T. A. Hyde, et al. Ind. Eng. Chem. Res., 2002, 41, 1425.
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Original Russian Text © 2018 M. B. Shavelkina, R. Kh. Amirov, N. R. Alikhanov, I. R. Vakhitov, T. B. Shatalova.
Translated from Zhurnal Strukturnoi Khimii, Vol. 59, No. 4, pp. 807–813, May-June, 2018
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Shavelkina, M.B., Amirov, R.K., Alikhanov, N.R. et al. Continuous Synthesis of Hydrogenated Graphene in Thermal Plasma. J Struct Chem 59, 773–779 (2018). https://doi.org/10.1134/S0022476618040042
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DOI: https://doi.org/10.1134/S0022476618040042