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Osmium Dimethyl Sulfoxide Complexes. Crystal Structure of the Complex [H(DMSO)2][OsIIIBr4(DMSO)2]

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Abstract

X-ray diffraction is used to study complex [H(DMSO)2][OsBr4(DMSO)2] (1). The compound crystallizes in the triclinic crystal system, space group Pī, unit cell parameters are as follows: a = 8.5942(3) Å, b = 8.7621(3) Å, c = 16.0193(6) Å, V = 1072.25(7) Å3, α = 76.3740(10)°, β = 75.6060(10)°, γ = 68.3790(10)°, Z = 2, R = 0.0270.

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Correspondence to O. V. Rudnitskaya.

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Original Russian Text © 2018 O. V. Rudnitskaya, E. K. Kultyshkina, E. V. Dobrokhotova, I.V. Ananyev.

Translated from Zhurnal Strukturnoi Khimii, Vol. 59, No. 3, pp. 696–698, March-April, 2018.

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Rudnitskaya, O.V., Kultyshkina, E.K., Dobrokhotova, E.V. et al. Osmium Dimethyl Sulfoxide Complexes. Crystal Structure of the Complex [H(DMSO)2][OsIIIBr4(DMSO)2]. J Struct Chem 59, 673–675 (2018). https://doi.org/10.1134/S0022476618030253

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  • DOI: https://doi.org/10.1134/S0022476618030253

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