Abstract
We present the results of studying the structure of gold nanoparticles synthesized on the silicon surface by two techniques: pulsed laser ablation and magnetron sputtering. The surface morphology is examined by scanning electron microscopy. The structure of the obtained gold nanoparticles is analyzed by transmission electron microscopy and electron diffraction. It is shown that nanoparticle sizes and crystal structures can be controlled by their thermal annealing. Mechanisms occurring during annealing of thin gold films and also their effect on the formation of nanoparticles with different structures are investigated.
Similar content being viewed by others
References
G. B. Sergeev, Nanochemistry [in Russian], 2nd ed., Izd. MGU, Moscow (2007).
M. Haruta, Chem. Rec. 3, No. 2, 75–87 (2003).
M. Turner, V. B. Golovko, O. P. H. Vaughan, et al., Nature, 454, 981–983 (2008).
M. Okumura, S. Nakamura, S. Tsubota, et al., Catal. Lett., 51, 53–58 (1998).
V. Amendola, M. Meneghetti, M. Stener, et al., Gold Nanoparticles in Analytical Chemistry, 66, Chapter 3, 81–152 (2014).
M. Haruta, Catal. Today 36, 153–166 (1997).
Y. Sun, L. Zhuang, J. Lu, X. Hong, and P. Liu, J. Am. Chem. Soc., 129, 15465–15467 (2007).
A. V. Bulgakov, N. M. Bulgakova, N. M. Burakov, et al., Synthesis of Nanosized Materials in the Interaction of Powerful Energy Fluxes on a Substance [ in Russian], Institute of thermophysics, Siberian Branch, Russian Academy of Sciences, Novosibirsk (2009).
S. V. Starinskii, Yu. G. Shukhov, and A. V. Bulgakov, Tech. Phys. Lett. 42, No. 4, 411–414 (2016).
K. K. S. Lau, Y. Mao, H. G. P. Lewis, et al., Thin Solid Films, 501, 211–215 (2006).
A. I. Safonov, V. S. Sulyaeva, N. I. Timoshenko, et al., Phys. Lett. A, 380, 3919–3923 (2016).
A. I. Safonov, V. S. Sulyaeva, N. I. Timoshenko, and S. V. Starinskiy, Thin Solid Films 603, 313–316 (2016).
A. I. Safonov, V. S. Sulyaeva, and N. I. Timoshenko, MATEC Web Conf., 37:01047, 1–5 (2015).
V. Švorčík, O. Kvítek, O. Lyutakov, et al., Appl. Phys. A, 102, 747–751 (2011).
P. Malinský, P. Slepička, V. Hnatowicz, and V. Švorčík, Nanoscale Res. Lett., 7:241, 1–7 (2012).
N. O. Krivulin, A. V. Pirogov, D. A. Pavlov, and A. I. Bobrov, FTP, 49, No. 2, 160–162 (2015).
L. I. Mirkin, Handbook on X-ray Diffraction Analysis of Polycrystals [in Russian]. GFML, Moscow (1961).
M. Janecek and R. Kral, Modern Electron Microscopy in Physical and Life Sciences, InTech (2016).
C. Polop, C. Rosiepen, S. Bleikamp, et al., New J. Phys., 9:74, 1–19 (2007).
R. Koch, J. Phys. Condens. Matter., 6, 9519–9550 (1994).
K. Oura, V. G. Lifshits, A. A. Saranin, et al., Introduction to Surface Physics [in Russian], Nauka, Moscow (2006).
A. B. Tesler, B. M. Maoz, Y. Feldman, et al., J. Phys. Chem. C, 117, No. 21, 11337–11346 (2013).
C. V. Thompson, Ann. Rev. Mater. 42, 399–434 (2012).
W. Kan and H. Wong, J. Appl. Phys., 97:043515, 1–9 (2005).
P. Jacquet, R. Podor, J. Ravaux, et al., Scr. Mater., 115, 128–132 (2016).
A. Vaskevich and I. Rubinstein, Phys. Chem. Chem. Phys. 15, 23–28 (2013).
A. T. Delariva, T. W. Hansen, S. R. Challa, and A. K. Datye, J. Catal., 308, 291–305 (2013).
I. Ozerov, A. V. Bulgakov, D. K. Nelson, et al., Appl. Surf. Sci., 247, 1–7 (2005).
A. V. Bulgakov, M. R. Predtechensky, and A. P. Mayorov, Appl. Surf. Sci., 96-98, 159–163 (1996).
E. Irissou, B. Le Drogoff, M. Chaker, et al., Appl. Phys. Lett., 80, 1716–1718 (2002).
T. W. Hansen, A. T. Delariva, S. R. Challa, and A. K. Datye, Acc. Chem. Res. 46, No. 8, 1720–1730 (2013).
M. Bechelany, X. Maeder, J. Riesterer, et al., Cryst. Growth Des., 10, No. 2, 587–596 (2010).
W. W. Mullins, J. Appl. Phys., 28, No. 3, 333–339 (1957).
P. Buffat and J. P. Borel, Phys. Rev. A 13, No. 6, 2287–2298 (1976).
R. T. K. Baker, P. S. Harris, and R. B. Thomas, Surf. Sci. 46, 311–316 (1974).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © 2017 S. V. Starinskiy, V. S. Sulyaeva, Yu. G. Shukhov, A. G. Cherkov, N. I. Timoshenko, A. V. Bulgakov, A. I. Safonov.
Translated from Zhurnal Strukturnoi Khimii, Vol. 58, No. 8, pp. 1631-1637, November-December, 2017.
Rights and permissions
About this article
Cite this article
Starinskiy, S.V., Sulyaeva, V.S., Shukhov, Y.G. et al. Comparison of structures of gold nanoparticles synthesized by pulsed laser ablation and magnetron sputtering. J Struct Chem 58, 1581–1587 (2017). https://doi.org/10.1134/S0022476617080157
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0022476617080157