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Structure and magnetic properties of pure and samarium doped magnetite nanoparticles

  • Applications of Synchrotron Radiation in Structural Chemistry
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Abstract

In this paper, a study of pure and doped samarium magnetite nanoparticles synthesized using a microwave synthesis in aqueous solution was performed. The shape, size and structure of the pure and samarium doped magnetite nanoparticles were determined by X-ray diffraction, transmission electron microscopy, X-ray absorption spectroscopy and Mössbauer spectroscopy. The magnetic properties of the nanoparticles were investigated using a vibrating sample magnetometer. It was found that the samarium doped magnetite nanoparticles were superparamagnetic with high saturation magnetization. The doping with a small amount of samarium allowed to reduce the size of nanoparticles, their size distribution, increase resistance to oxidation and improve their magnetic characteristics.

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Authors and Affiliations

  1. Southern Federal University, Rostov-on-Don, Russia

    O. E. Polozhentsev, V. V. Butova, V. K. Kochkina & A. V. Soldatov

  2. Research Institute of Physics, Southern Federal University, Rostov-on-Don, Russia

    S. P. Kubrin & V. V. Stashenko

Authors
  1. O. E. Polozhentsev
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  2. S. P. Kubrin
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  3. V. V. Butova
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  4. V. K. Kochkina
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  5. A. V. Soldatov
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  6. V. V. Stashenko
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Correspondence to O. E. Polozhentsev.

Additional information

Translated from Zhurnal Strukturnoi Khimii, Vol. 57, No. 7, pp. 1539-1549, September-October, 2016.

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Polozhentsev, O.E., Kubrin, S.P., Butova, V.V. et al. Structure and magnetic properties of pure and samarium doped magnetite nanoparticles. J Struct Chem 57, 1459–1468 (2016). https://doi.org/10.1134/S0022476616070222

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  • DOI: https://doi.org/10.1134/S0022476616070222

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