Skip to main content
Log in

Research on fast solid-state chemical reactions at the Siberian Synchrotron and Terahertz Radiation Center

  • Applications of Synchrotron Radiation in Structural Chemistry
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

The potent equipment of the shared-use center “Siberian Synchrotron and Terahertz Radiation Center” at Budker Institute of Nuclear Physics of the Siberian Branch of the Russian Academy of Sciences (BINP SB RAS) enables conduction of time-resolved X-ray diffraction experiments using synchrotron radiation of the VEPP-3/VEPP-4 storage rings. These experiments are performed mostly for institutions of the Siberian Branch of the Russian Academy of Sciences (SB RAS). The experiments yielded novel techniques, which have been implemented for investigation into the dynamics of the nucleation and formation of nanoparticles under explosion and shock wave impact with a nanosecond-scale time resolution (the X-ray exposure time is 73 ps), dynamics of structural transformations in chemical reactions, and kinetics of chemical reactions during gasless combustion (SHS) with a millisecond-scale time resolution, obtaining structural information about the state of catalysts and so on.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. O. V. Evdokov, V. M. Titov, B. P. Tolochko, and M. R. Sharafutdinov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 194–195 (2009).

    Article  CAS  Google Scholar 

  2. V. Bessergenev and B. P. Tolochko, Nucl. Instrum. Methods Phys. Res., Sect. A, 359, 160–164 (1995).

    Article  CAS  Google Scholar 

  3. N. Aleshaev, A. M. Batrakov, M. G. Fedotov, G. N. Kulipanov, L. A. Luckjanchikov, N. Z. Lyachov, S. I. Mishnev, M. A. Sheromov, K. A. Ten, V. M. Titov, B. P. Tolochko, and P. I. Zubkov, Nucl. Instrum. Methods Phys. Res., Sect. A, 470, Nos. 1/2, 240–244 (2001).

    Article  CAS  Google Scholar 

  4. N. Aleshaev, P. I. Zubkov, G. N. Kulipanov, L. A. Luk'yanchikov, N. Z. Lyakhov, S. I. Mishnev, K. A. Ten, V. M. Titov, B. P. Tolochko, M. G. Fedotov, and M. A. Sheromov, Fiz. Goreniya Vzryva, 37, No. 5, 104–113 (2001).

    Google Scholar 

  5. P. Tolochko, A. N. Aleshaev, M. G. Fedotov, G. N. Kulipanov, N. Z. Lyakhov, L. A. Luk'yanchikov, S. I. Mishnev, M. A. Sheromov, K. A. Ten, V. M. Titov, and P. I. Zubkov, Nucl. Instrum. Methods Phys. Res., Sect. A, 467/468, Part 2, 990–993 (2001).

    Article  Google Scholar 

  6. M. Bagge-Hansen, L. Lauderbach, R. Hodgin, S. Bastea, L. Fried, A. Jones, T. van Buuren, D. Hansen, J. Benterou, C. May, T. Graber, B. J. Jensen, J. Ilavsky, and T. M. Willey, J. Appl. Phys., 117, 245902 (2015).

  7. K. A. Ten, E. R. Pruuel, L. A. Merzhievsky, L. A. Lukjanchikov, B. P. Tolochko, I. L. Zhogin, and L. I. Shekhtman, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 160–163 (2009).

    Article  CAS  Google Scholar 

  8. E. R. Pruuel, K. A. Ten, V. M. Titov, L. A. Lukianchikov, L. A. Merzhievsky, P. I. Zubkov, B. P. Tolochko, I. L. Zhogin, V. V. Zhulanov, V. M. Aulchenko, and L. I. Shekhtman, Proc. 14th Int. Detonation Symposium (IDS) (2010), p. 345–351.

    Google Scholar 

  9. V. M. Titov, E. R. Pruuél, K. A. Ten, L. A. Luk'yanchikov, L. A. Merzhievskii, B. P. Tolochko, V. V. Zhulanov, and L. I. Shekhtman, Combust., Explos. Shock Waves, 47, No. 6, 615–626 (2011).

    Article  Google Scholar 

  10. V. V. Milyavskiy, K. A. Ten, T. I. Borodina, L. A. Lukianchikov, E. R. Pruuel, V. V. Zhulanov, and B. P. Tolochko, J. Appl. Sci, 11, No. 7, 1453–1456 (2011).

  11. L. A. Merzhievsky, E. V. Bespalov, V. P. Efremov, L. A. Lukianchikov, E. R. Pruuel, K. A. Ten, V. M. Titov, B. P. Tolochko, V. E. Fortov, and M. R. Sharafutdinov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 164–166 (2009).

    Article  CAS  Google Scholar 

  12. N. Shmakov and Z. A. Vinokurov, J. Struct. Chem., in press (2016).

    Google Scholar 

  13. V. M. Aulchenko, V. D. Kutovenko, V. M. Titov, A. V. Vasiljev, V. V. Zhulanov, O. V. Evdokov, B. Ya. Pirogov, M. R. Sharafutdinov, B. P. Tolochko, and I. A. Zhogin, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 76–79 (2009).

    Article  CAS  Google Scholar 

  14. A. I. Ancharov, A. Yu. Manakov, N. A. Mezentsev, B. P. Tolochko, M. A. Sheromov, and V. M. Tsukanov, Nucl. Instrum. Methods Phys. Res., Sect. A, 470, Nos. 1/2, 80–83 (2001).

    Article  CAS  Google Scholar 

  15. M. Sharafutdinov, V. Alexandrov, O. Evdokov, D. Naumov, B. Pirogov, E. Pismenskaya, A. Rogachev, and B. Tolochko J. Synchrotron Radiat., 10, No. 5, 384–386 (2003).

    Article  CAS  Google Scholar 

  16. M. R. Sharafutdinov, M. A. Korchagin, N. F. Shkodich, B. P. Tolochko, P. A. Tsygankov, and I. Yu. Yagubova, Nucl. Instrum. Methods Phys. Res., Sect. A, 575, Nos. 1/2, 149–151 (2007).

    Article  CAS  Google Scholar 

  17. S. Rogachev, J.-C. Gachon, H. E. Grigoryan, E. Illeková, N. F. Kochetov, F. N. Nosyrev, N. V. Sachkova, J. C. Schuster, M. R. Sharafutdinov, N. F. Shkodich, B. P. Tolochko, P. A. Tsygankov, and I. Y. Yagubova, Nucl. Instrum. Methods Phys. Res., Sect. A, 575, Nos. 1/2, 126–129 (2007).

    Article  CAS  Google Scholar 

  18. N. F. Shkodich, N. A. Kochetov, A. S. Rogachev, A. E. Grigoryan, M. R. Sharafutdinov, and B. P. Tolochko, Bull. Russ. Acad. Sci.: Phys., 71, No. 5, 650–652 (2007).

    Article  Google Scholar 

  19. Yu. Yagubova, A. E. Grigoryan, A. S. Rogachev, M. R. Sharafutdinov, B. P. Tolochko, P. A. Tsygankov, and A. N. Nosyrev, Bull. Russ. Acad. Sci.: Phys., 71, No. 2, 270–271 (2007).

    Article  Google Scholar 

  20. A. S. Rogachev, B. P. Tolochko, N. Z. Lyakhov, M. P. Sharafutdinov, N. A. Popkov, B. Ya. Pirogov, and E. B. Pis'menskaya, Crystallogr. Rep., 48, No. 3, 466–468 (2003).

    Article  CAS  Google Scholar 

  21. A. S. Rogachev, B. P. Tolochko, N. Z. Lyakhov, M. P. Sharafutdinov, N. A. Popkov, B. Ya. Pirogov, E. B. Pis'menskaya, Kristallografiya, 48, No. 3, 511–514 (2003).

    Google Scholar 

  22. M. G. Fedotov, G. N. Kulipanov, L. A. Luckjanchikov, N. Z. Lyakhov, M. R. Sharafutdinov, M. A. Sheromov, K. A. Ten, V. M. Titov, B. P. Tolochko, and P. I. Zubkov, Nucl. Instrum. Methods Phys. Res., Sect. A, 470, Nos. 1/2, 245–248 (2001).

    Article  CAS  Google Scholar 

  23. O. V. Evdokov, M. G. Fedotov, G. N. Kulipanov, L. A. Luckjanchikov, N. Z. Lyakhov, S. I. Mishnev, M. R. Sharafutdinov, M. A. Sheromov, K. A. Ten, V. M. Titov, B. P. Tolochko, and P. I. Zubkov, Nucl. Instrum. Methods Phys. Res., Sect. A, 470, Nos. 1/2, 236–239 (2001).

    Article  CAS  Google Scholar 

  24. B. P. Tolochko, V. M. Titov, A. P. Chernyshev, K. A. Ten, E. R. Pruuel, I. L. Zhogin, P. I. Zubkov, N. Z. Lyakhov, L. A. Lukyanchikov, and M. A. Sheromov, Diamond Relat. Mater., 16, No. 12, 2014–2017 (2007).

    Article  CAS  Google Scholar 

  25. K. A. Ten, V. M. Aulchenko, L. A. Lukjanchikov, E. R. Pruuel, L. I. Shekhtman, B. P. Tolochko, I. L. Zhogin, and V. V. Zhulanov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 102–104 (2009).

    Article  CAS  Google Scholar 

  26. K. A. Ten, V. M. Titov, E. R. Pruuel, L. A. Lukyanchikov, B. P. Tolochko, I. L. Zhogin, Y. A. Aminov, V. P. Filin, B. G. Loboyko, A. K. Muzyrya, and E. B. Smirnov, Proc. 14th Int. Detonation Symposium (IDS) (2010), p. 387–391.

    Google Scholar 

  27. V. M. Titov, B. P. Tolochko, K. A. Ten, L. A. Lukyanchikov, and E. R. Pruuel, Diamond Relat. Mater., 16, No. 12, 2009–2013 (2007).

    Article  CAS  Google Scholar 

  28. B. P. Tolochko, A. P. Chernyshev, K. A. Ten, E. R. Pruuel, I. L. Zhogin, P. I. Zubkov, N. Z. Lyakhov, L. A. Luk'yanchikov, and M. A. Sheromov, Phys. Met. Metallogr., 105, No. 2, 134–140 (2008).

    Google Scholar 

  29. A. N. Shmakov, Complex Diagnostics of Structure of Materials Using SR X-Ray Diffraction Methods, Doctoral (Phys.-Math.) Dissertation, Novosibirsk (2015).

    Google Scholar 

  30. E. G. Kodenev, A. N. Shmakov, A. Yu. Derevyankin, O. B. Lapina, and V. N. Romannikov, J. Mol. Catal. A: Chem., 158, No. 1, 349–354 (2000).

    Article  CAS  Google Scholar 

  31. O. A. Kholdeeva, A. Yu. Derevyankin, A. N. Shmakov, N. N. Trukhan, E. A. Paukshtis, A. Tuel, and V. N. Romannikov, J. Mol. Catal. A: Chem., 158, No. 1, 417–421 (2000).

    Article  CAS  Google Scholar 

  32. V. N. Romannikov, S. D. Kirik, L. A. Solov'ev, A. N. Shmakov, A. Yu. Derevyankin, V. B. Fenelonov, O. A. Holdeeva, O. B. Lapina, and E. A. Paukshtis, Kinet. Catal., 42, No. 6, 359–368 (2001).

    Article  Google Scholar 

  33. V. B. Fenelonov, A. Yu. Derevyankin, S. D. Kirik, L. A. Solovyov, A. N. Shmakov, J.-L. Bonardet, A. Gedeon, and V. N. Romannikov, Microporous Mesoporous Mater., 44/45, 33–40 (2001).

    Article  Google Scholar 

  34. L. A. Solovyov, S. D. Kirik, A. N. Shmakov, and V. N. Romannikov, Microporous Mesoporous Mater., 44/45, 17–23 (2001).

    Article  Google Scholar 

  35. L. A. Solovyov, A. N. Shmakov, V. I. Zaikovskii, S. H. Joo, and R. Ryoo, Carbon, 40, No. 13, 2477–2481 (2002).

    Article  CAS  Google Scholar 

  36. E. A. Mel'gunova, Yu. M. Balabina, A. N. Shmakov, and M. S. Mel'gunov, J. Phys. Chem., 77, No. 3, 444–448 (2003).

    Google Scholar 

  37. I. I. Simentsova, A. A. Hasin, T. P. Minyukova, L. P. Davydova, A. N. Shmakov, O. A. Bulavchenko, S. V. Cherepanova, G. N. Kustova, and T. M. Yur'eva, Kinet. Catal., 53, No. 4, 520–526 (2012).

    Article  Google Scholar 

  38. A. N. Shmakov and O. Yu. Podyacheva, J. Struct. Chem., 55, No. 4, 791–798 (2014).

    Article  CAS  Google Scholar 

  39. O. Yu. Podyacheva, Z. R. Ismagilov, A. N. Shmakov, M. G. Ivanov, A. N. Nadeev, S. V. Tsybulya, and V. A. Rogov, Catal. Today, 147, Nos. 3/4, 270–274 (2009).

    Article  CAS  Google Scholar 

  40. M. G. Ivanov, A. N. Shmakov, V. A. Drebushchak, and O. Yu. Podyacheva, J. Therm. Anal. Calorim., 100, No. 1, 79–82 (2010).

    Article  CAS  Google Scholar 

  41. M. G. Ivanov, A. N. Shmakov, S. V. Tsybulya, O. Yu. Podyacheva, and Z. R. Ismagilov, Solid State Phenom., 163, 38–41 (2010).

    Article  CAS  Google Scholar 

  42. M. G. Ivanov, A. N. Shmakov, O. Yu. Podyacheva, and Z. R Ismagilov, J. Struct. Chem., 51, S47–S52 (2010).

    Article  Google Scholar 

  43. O. Yu. Podyacheva, Z. R. Ismagilov, A. E. Shalagina, V. A. Ushakov, A. N. Shmakov, S. V. Tsybulya, V. V. Kriventsov, and A. V. Ischenko, Carbon, 48, No. 10, 2792–2801 (2010).

    Article  CAS  Google Scholar 

  44. O. Yu. Podyacheva, A. N. Shmakov, A. I. Boronin, L. S. Kibis, S. V. Koscheev, E. Yu. Gerasimov, and Z. R. Ismagilov, J. Energy Chem., 22, No. 2, 270–279 (2013).

    Article  CAS  Google Scholar 

  45. O. Yu. Podyacheva, A. N. Shmakov, and Z. R. Ismagilov, Carbon, 52, 486–492 (2013).

    Article  CAS  Google Scholar 

  46. O. Yu. Podyacheva, A. N. Shmakov, Z. R. Ismagilov, and V. N. Parmon, Proc. Acad. Sci., 439, No. 1, 72–75 (2011).

    Google Scholar 

  47. X-Ray Diffraction of Catalysts Under Controlled Conditions of Temperature and Environment [in Russian], L. M. Plyasova (ed.), Publ. House of the Institute of Catalysis SB RAS, Novosibirsk (2011).

  48. N. A. Timchenko, R. M. Galimov, A. N. Shmakov, A. M. Lider, and I. N. Chernov, Izv. Vyssh. Ucheb. Zaved., Fiz., 54, No. 11 (2), 190–194 (2011).

    Google Scholar 

  49. N. V. Kosova, E. T. Devyatkina, A. I. Ancharov, A. V. Markov, D. D. Karnaushenko, and V. K. Makukha, Solid State Ionics, 225, 564–569 (2012).

    Article  CAS  Google Scholar 

  50. B. P. Tolochko, A. I. Maslii, and M. A. Sheromov, Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, No. 1, 48–54 (1985).

    Google Scholar 

  51. N. Z. Lyakhov, A. I. Maslii, B. P. Tolochko, and M. A. Sheromov, Nucl. Instrum. Methods Phys. Res., Sect. A, 261, Nos. 1/2, 209–215 (1987).

    Article  Google Scholar 

  52. B. P. Tolochko, A. I. Maslii, and N. Z. Lyakhov, Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, No. 1, 54–58 (1985).

    Google Scholar 

  53. M. R. Sharafutdinov, B. P. Tolochko, and N. Z. Lyakhov, Nucl. Instrum. Methods Phys. Res., Sect. A, 470, Nos. 1/2, 228–231 (2001).

    Article  CAS  Google Scholar 

  54. E. G. Avvakumov, Mechanochemical Methods of Activation of Chemical Processes [in Russian], Nauka, Novosibirsk (1986).

    Google Scholar 

  55. O. V. Evdokov, V. M. Titov, B. P. Tolochko, and M. R. Sharafutdinov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 194–195 (2009).

    Article  CAS  Google Scholar 

  56. V. M. Zhukovsky and A. N. Petrov, J. Appl. Chem., 46, No. 10, 2159–2162 (1973).

    Google Scholar 

  57. E. V. Tkachenko and V. M. Zhukovsky, J. Appl. Chem., 46, No. 10, 2129–2134 (1973).

    CAS  Google Scholar 

  58. V. V. Boldyrev, N. Z. Lyakhov, B. P. Tolochko, et al., Diffractometry Using Synchrotron Radiation [in Russian], G. N. Kulipanov (ed.), Nauka, Novosibirsk (1989).

  59. A. V. Besserguenev, B. P. Tolochko, M. A. Sheromov, and N. A. Mezenchev, Nucl. Instrum. Methods Phys. Res., 359, 160–164 (1995).

    Article  Google Scholar 

  60. L. Kihlborg, Adv. Chem., 39, No. 3, 37–45 (1963).

    Article  CAS  Google Scholar 

  61. G. Swensson and L. Kihlborg, React. Solids, 3, 33–43 (1987).

    Article  Google Scholar 

  62. A. V. Bessergenev and B. P. Tolochko, Nucl. Instrum. Methods Phys. Res., Sect. A, 356, 160 (1995).

    Article  Google Scholar 

  63. B. B. Bokhonov, M. R. Sharafutdinov, B. P. Tolochko, L. P. Burleva, and D. R. Whitcomb, J. Imaging Sci. Technol., 51, No. 4, 386–390 (2007).

    Article  CAS  Google Scholar 

  64. B. B. Bokhonov, M. R. Sharafutdinov, D. R. Whitcomb, and L. P. Burleva, J. Phys. Chem. C, 118, No. 22, 11980–11989 (2014).

    Article  CAS  Google Scholar 

  65. A. I. Ancharov, T. F. Grigorieva, S. G. Nikitenko, and M. R. Sharafutdinov, Poverkhnost, No. 7, 25–28 (2002).

    Google Scholar 

  66. A. I. Ancharov and T. F. Grigorieva, Nucl. Instrum. Methods Phys. Res., A543, 139–142 (2005).

  67. A. I. Ancharov, T. F. Grigorieva, S. V. Tsybulya, and V. V. Boldyrev, Inorg. Mater., 42, No. 10, 1164–1170 (2006).

    Article  Google Scholar 

  68. A. I. Ancharov, T. F. Grigorieva, S. V. Tsybulya, and V. V. Boldyrev, Metals, No. 2, 55–59 (2006).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to B. P. Tolochko.

Additional information

Translated from Zhurnal Strukturnoi Khimii, Vol. 57, No. 7, pp. 1362-1388, September-October, 2016.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Tolochko, B.P., Zolotarev, K.V. Research on fast solid-state chemical reactions at the Siberian Synchrotron and Terahertz Radiation Center. J Struct Chem 57, 1288–1313 (2016). https://doi.org/10.1134/S0022476616070027

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476616070027

Keywords

Navigation