Skip to main content
SpringerLink
Log in

X-ray crystallographic study of 2-morpholino-5-trifluoromethyl-1,3,4-thiadiazole

  • Brief Communications
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

By single crystal X-ray diffraction the features of the molecular and crystal structures of 2-morpholino- 5-trifluoromethyl-1,3,4-thiadiazole are determined. This is the main substance of the certified reference material of trifluoromethylmorpholinothiadiazole for the quantitative elemental analysis of fluoroorganic compounds.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. L. N. Bazhenova, V. E. Kirichenko, E. V. Letova, et al., Proc. of the 13th Conf. “High-Purity Compounds and Materials. Synthesis, analysis, application” [in Russian], N. Novgorod (2007). p. 128.

    Google Scholar 

  2. Certificate No. 3459/1 on Recognition of the Type of State Certified Reference Material (SCRM), Regist. number according to Nat. Register of Russia: SCRM 8853-2007, State Register of Federal Agency on Technical Regulation and Metrology, М. (2007).

  3. Certificate No. 3459 on Recognition of the Type of the Interstate Certified Reference Material (CIS CRM), Regist. number according to Interstate Register: CIS CRM 1368-2007, Interstate Register of Certified Reference Materials of Composition and Properties of Substances and Materials of the States-Participants of Agreement on Policy Coherence in the Field of Standardization, Metrology and Certification, Minsk (2007).

  4. International Data Bank of the Interstate Certified Reference Material Properties of Substances and Materials, The Central Secretariat in Berlin, Germany.

  5. E. B. Vasil`eva, V. I. Filyakova, L. P. Sidorova, et al., Russ. J. Org. Chem., 41, No. 10, 1522 (2005).

    Article  CAS  Google Scholar 

  6. G. M. Sheldrick, Acta Crystallogr., A64, 112 (2008).

    Article  Google Scholar 

  7. International Tables for Crystallography, vol. C (2006). chap. 9.5, pp. 790–811.

Download references

Author information

Authors and Affiliations

  1. Postovsky Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, Ekaterinburg, Russia

    P. A. Slepukhin, L. N. Bazhenova, E. B. Letova & V. I. Filyakova

Authors
  1. P. A. Slepukhin
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. L. N. Bazhenova
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. E. B. Letova
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. I. Filyakova
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to V. I. Filyakova.

Additional information

Original Russian Text © 2015 P. A. Slepukhin, L. N. Bazhenova, E. B. Letova, V. I. Filyakova.

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 7, pp. 1471/1472, November-December, 2015.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Slepukhin, P.A., Bazhenova, L.N., Letova, E.B. et al. X-ray crystallographic study of 2-morpholino-5-trifluoromethyl-1,3,4-thiadiazole. J Struct Chem 56, 1415–1416 (2015). https://doi.org/10.1134/S0022476615070252

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476615070252

Keywords

Search

Navigation