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Structure and thermal properties of the molybdenum complex Mo(acac)3

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Abstract

A method for the synthesis of the Mo(acac)3 complex is proposed and its crystal structure is determined by single crystal X-ray diffraction. Space group P21/c, a = 19.7538(5) Å, b = 7.4821(2) Å, c = 34.6190(8) Å, β = 96.8055(12)°, V = 5080.6(2) Å3, Z = 12. The compound is studied by the thermogravimetric analysis, and MoO3 is shown to be the result of its decomposition.

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Authors and Affiliations

  1. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    A. Yu. Ledneva, S. B. Artemkina, D. A. Piryazev & V. E. Fedorov

  2. Novosibirsk National Research State University, Novosibirsk, Russia

    S. B. Artemkina & V. E. Fedorov

Authors
  1. A. Yu. Ledneva
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  2. S. B. Artemkina
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  3. D. A. Piryazev
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  4. V. E. Fedorov
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Correspondence to A. Yu. Ledneva.

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Original Russian Text © 2015 A. Yu. Ledneva, S. B. Artemkina, D. A. Piryazev, V. E. Fedorov.

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Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 5, pp. 1079–1081, September–October, 2015.

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Ledneva, A.Y., Artemkina, S.B., Piryazev, D.A. et al. Structure and thermal properties of the molybdenum complex Mo(acac)3 . J Struct Chem 56, 1021–1023 (2015). https://doi.org/10.1134/S0022476615050315

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  • DOI: https://doi.org/10.1134/S0022476615050315

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