Abstract
The X-ray crystallographic analysis of benzoaza-12-crown-4 hydrochloride crystals is performed for the first time: space group P1, a = 7.7497(4) Å, b = 9.2224(5) Å, c = 10.2395(5) Å, α = 99.3965(10)°, β = 101.8387(11)°, γ = 112.6470(10)°, V = 636,81(6) Å3, Z = 2, ρcalc = 1.355 g/cm3. The conformation of the 12-membered ring of the molecule is determined.
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Original Russian Text © 2015 V. N. Glushko, N. Yu. Sadovskaya, L. I. Blokhina, I. V. Anan‘ev.
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Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 1, pp. 149–154, January–February, 2015.
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Glushko, V.N., Sadovskaya, N.Y., Blokhina, L.I. et al. Crystal and molecular structure of benzoaza-12-crown-4 hydrochloride. J Struct Chem 56, 142–147 (2015). https://doi.org/10.1134/S0022476615010205
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DOI: https://doi.org/10.1134/S0022476615010205