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Molecular and crystal structure of ethyl-3(allylamino)-9,9-dimethyl-7,11-dioxo-1,5-diphenylspiro [5.5]undec-2-en-2-carboxylate

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Abstract

New multicomponent condensation of dimedone, benzaldehyde, acetacetic ester, and allylamine in the 1:2:1:1 molar ratio respectively is revealed. It proceeds with the formation of ethyl-3(allylamino)-9,9-dimethyl-7,11-dioxo-1.5-diphenyl-spiro[5.5]undec-2-en-2-carboxylate whose crystal structure is determined by single crystal X-ray diffraction.

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Correspondence to A. I. Ismiev.

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Original Russian Text © 2014 A. M. Magerramov, A. I. Ismiev, K. A. Potekhin, R. K. Askerov.

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Translated from Zhurnal Strukturnoi Khimii, Vol. 55, No. 1, pp. 155–157, January–February, 2014.

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Magerramov, A.M., Ismiev, A.I., Potekhin, K.A. et al. Molecular and crystal structure of ethyl-3(allylamino)-9,9-dimethyl-7,11-dioxo-1,5-diphenylspiro [5.5]undec-2-en-2-carboxylate. J Struct Chem 55, 151–153 (2014). https://doi.org/10.1134/S0022476614010260

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  • DOI: https://doi.org/10.1134/S0022476614010260

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