Skip to main content
SpringerLink
Log in

Structural analysis of ethyl 2-Z-phenylhydrazono-3-E-methylthio(thioxo)methylhydrazone-butanoate

  • Brief Communications
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

A new compound of ethyl 2-Z-phenylhydrazono-3-E-methylthio(thioxo) methylhydrazone-butanoate is synthesized via the reaction between ethyl 2-Z-phenylhydrazono-3-oxo-butanoate and S-methyldithio-carbazate at room temperature. A single crystal of the titled compound is obtained and the structure is determined by X-ray diffraction. It belongs to a monoclinic P21 space group with the cell parameters: a = 5.335(1) Å, b = 15.907(4) Å, c = 9.507(2) Å, β = 90.21(1)°, V = 806.8(4) Å3. A one-dimensional parallel structure is constructed by an unclassic hydrogen bond and a weak p-π interaction.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. P. Bandyopadhyay, L. Guha, T. Seenivasagan, M. Sathe, B. D. Parashar, M. P. Kaushik, and P. Sharma, Bioorg. Med. Chem. Lett., 21, 794 (2011)

    Article  CAS  Google Scholar 

  2. F.-X. Li, T.-X. Liu, Y.-S. Huang, and G.-W. Wang, J. Org. Chem., 74, 7743 (2009)

    Article  CAS  Google Scholar 

  3. Y.-S. Huang, L. Taylor, X. Chen, and N. Ayres, J. Polym. Sci. A Poly. Chem., 51, 5230 (2013).

    Article  CAS  Google Scholar 

  4. G. N. Ferguson, C. Valant, J. Horne, B. L. Flynn, D. K. Chalmers, P. M. Sexton, P. J. Scammells, A. Christopoulos, H. Figler, and J. Linden, J. Med. Chem., 51, 6165 (2008).

    Article  CAS  Google Scholar 

  5. T. D. Lash, K. A. Bladel, C. M. Shiner, D. L. Zajeski, and R. P. Balasubramaniam, J. Org. Chem., 57, 4809 (1992).

    Article  CAS  Google Scholar 

  6. P. S. Shinge, P. R. Latthe, and B. V. Badami, Syn. Commun., 35, 2169 (2005).

    Article  CAS  Google Scholar 

  7. A. M. Isloor, B. Kalluraya, and K. Sridhar Pai, Eur. J. Med. Chem., 45, 825 (2010).

    Article  CAS  Google Scholar 

  8. B. F. Abdel-Wahab, A. S. El-Ahl, and F. A. Badria, Chem. Pharm. Bull., 57, 1348 (2009).

    Article  CAS  Google Scholar 

  9. S. M. Gomha and S. M. Riyadh, Molecules, 16, 8244 (2011).

    Article  CAS  Google Scholar 

  10. M. A. A. Elneairy, M. A. M. Gad-Elkareem, and A. M. A. Abdel-Fattah, Phosphorus, Sulfur, and Silicon, 181, 1451 (2006).

    Article  CAS  Google Scholar 

  11. A. O. Abdelhamid, Z. H. Ismail, S. M. Abdel-Gawad, M. M. Ghorab, and A. Abdel-Aziem, Phosphorus, Sulfur, and Silicon, 184, 58 (2009).

    Article  CAS  Google Scholar 

  12. P. Wu, J. Struct. Chem., 54, 960 (2013).

    Article  CAS  Google Scholar 

  13. SAINT, Version 6.02a, Bruker AXS Inc., Madison, WI (2002).

  14. G. M. Sheldrick, SADABS, Program for Bruker Area Detector Absorption Correction, Univ. Göttingen, Germany (1997).

    Google Scholar 

  15. G. M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, Univ. Göttingen, Germany (1997)

    Google Scholar 

  16. G. M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, Univ. Göttingen, Germany (1997).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Chemistry, Dezhou College, Dezhou, Shandong, China

    P. Wu

Authors
  1. P. Wu
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to P. Wu.

Additional information

Original Russian Text © 2014 P. Wu.

The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 55, No. 1, pp. 151–154, January–February, 2014.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Wu, P. Structural analysis of ethyl 2-Z-phenylhydrazono-3-E-methylthio(thioxo)methylhydrazone-butanoate. J Struct Chem 55, 147–150 (2014). https://doi.org/10.1134/S0022476614010259

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476614010259

Keywords

Search

Navigation