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Supramolecular architecture of a 1:1 complex of pyrogallol with dimethylsulfoxide

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Abstract

The crystal structure is solved for a 1:1 molecular complex of pyrogallol and dimethylsulfoxide. Crystal data: C8H12O4S, M = 204.24, orthorhombic, Pna21 space group; unit cell parameters: a = 10.9620(4) Å, b = 10.9542(4) Å, c = 8.0561(3) Å, V = 967.38(6) Å3, Z = 4, d x = 1.402 g/cm3, R1 = 0.0216, T = 150 K. The molecules are joined in a supramolecular ensemble by O-H…O and C-H…π hydrogen bonds.

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Authors and Affiliations

  1. A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    T. M. Polyanskaya & A. I. Smolentsev

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  1. T. M. Polyanskaya
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  2. A. I. Smolentsev
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Correspondence to T. M. Polyanskaya.

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Original Russian Text Copyright © 2012 by T. M. Polyanskaya, A. I. Smolentsev

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Translated from Zhurnal Strukturnoi Khimii, Vol. 53, No. 3, pp. 574–579, May–June, 2012.

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Polyanskaya, T.M., Smolentsev, A.I. Supramolecular architecture of a 1:1 complex of pyrogallol with dimethylsulfoxide. J Struct Chem 53, 568–573 (2012). https://doi.org/10.1134/S0022476612030225

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  • DOI: https://doi.org/10.1134/S0022476612030225

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