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Structure and microstructure of nano-crystalline samples of the composition Re0.65Pt0.35

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Abstract

Alloys of the composition Re0.65Pt0.35 are prepared by thermal reduction of a bimetallic complex salt (NH4)2[ReCl6]0.65[PtCl6]0.35 in the hydrogen atmosphere and also by thermal-baric treatment of a mixture of nanosized powders of rhenium and platinum. The products are examined by powder X-ray diffraction and HRTEM. The compositions of the obtained phases are estimated using EDS and crystal chemical analysis of phases known for the Re-Pt system.

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References

  1. L. I. Voronova, V. P. Polyakova, and E. M. Savitskii, Metally, No. 1, 185–187 (1984).

  2. E. M. Savitskii, M. A. Tylkina, and K. B. Povarova, Rhenium Alloys [in Russian], Nauka, Moscow (1965).

    Google Scholar 

  3. W. Trzebiatowski and J. Berak, Bull. Acad. Polon. Sci., 2, No. 1, 35–38 (1954).

    Google Scholar 

  4. P. S. Rudman, J. Less-Common Met., 12, No. 1, 79–81 (1967).

    Article  CAS  Google Scholar 

  5. K. V. Yusenko, I. A. Baidina, S. A. Gromilov, and S. V. Korenev, J. Struct. Chem., 48, No. 3, 578–582 (2007).

    Article  CAS  Google Scholar 

  6. I. V. Korolkov, A. V. Zadesenets, S. A. Gromilov, K. V. Yusenko, I. A. Baidina, and S. V. Korenev, J. Struct. Chem., 47, No. 3, 489–498 (2006).

    Article  CAS  Google Scholar 

  7. E. Shusharina, A. Zadesenetz, and S. Gromilov, Acta Crystallogr., A65, S286/S287 (2009).

    Google Scholar 

  8. S. A. Gromilov, Yu. V. Shubin, E. Yu. Filatove, et al., J. Struct. Chem., 52, No. 3, 505–509 (2011).

    Article  CAS  Google Scholar 

  9. C. Bradley, High Pressure Methods in Solid State Research, Butterworth & Co Publishers Ltd (1968). Russian Translation Mir, Moscow (1972).

  10. W. Kraus and G. Nolze, J. Appl. Crystallogr., 29, 301–303 (1996).

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    E. A. Bykova, A. V. Zadesenets & S. A. Gromilov

  2. Research and Education Complex “Nanosystems and Modern Materials.”, Novosibirsk State University, Novosibirsk, Russia

    A. V. Zadesenets & S. A. Gromilov

  3. Institute of Solid State Chemistry, Ural Division, Russian Academy of Sciences, Ekaterinburg, Russia

    T. V. D’yachkova

  4. G. K. Boreskov Institute of Catalysis, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    E. Yu. Gerasimov

Authors
  1. E. A. Bykova
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  2. A. V. Zadesenets
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  3. T. V. D’yachkova
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  4. E. Yu. Gerasimov
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  5. S. A. Gromilov
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Corresponding author

Correspondence to S. A. Gromilov.

Additional information

Original Russian Text Copyright © 2012 by E. A. Bykova, A. V. Zadesenets, T. V. D’yachkova, E. Yu. Gerasimov, S. A. Gromilov

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Translated from Zhurnal Strukturnoi Khimii, Vol. 53, No. 3, pp. 563–568, May–June, 2012.

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Bykova, E.A., Zadesenets, A.V., D’yachkova, T.V. et al. Structure and microstructure of nano-crystalline samples of the composition Re0.65Pt0.35 . J Struct Chem 53, 557–562 (2012). https://doi.org/10.1134/S0022476612030201

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  • DOI: https://doi.org/10.1134/S0022476612030201

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